Hydrochloric Acid Treatment of InP Surfaces in N2-Controlled Atmosphere

The objective of this study is to investigate the oxide removal and the reoxidation mechanisms occurring on indium phosphide (InP) surfaces in a cleanroom environment after HCl wet treatments. For this purpose, an experimental setup was mounted, tuned and validated consisting of a glove box connected to a X-ray photoelectron spectroscopy (XPS) chamber, enabling quasi in-situ sample transfer after HCl wet treatment without any air exposure. We showed that a dip of at least 3 min in HCl with a concentration of at least 0.5% (0.137 mol/L) effectively removed indium phosphates (InPO x ) from InP surfaces. Reoxidation of HCl-treated InP surfaces was observed after more than 1 min of air exposure.

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Publication Details

Journal
Diffusion and defect data, solid state data. Part B, Solid state phenomena/Solid state phenomena
Published
2026-10-29
DOI
https://doi.org/10.4028/p-ixrbe3
Primary Topic
Semiconductor materials and devices
Type
article
Field-Weighted Citation Impact
0.00
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article

Hydrochloric Acid Treatment of InP Surfaces in N2-Controlled Atmosphere

Virginie Loup, Victor Lumineau, Bernard Pelissier, Georges Al Hoyek
Diffusion and defect data, solid state data. Part B, Solid state phenomena/Solid state phenomena
Semiconductor materials and devices
article

Hydrochloric Acid Treatment of InP Surfaces in N2-Controlled Atmosphere

Virginie Loup, Victor Lumineau, Bernard Pelissier, Georges Al Hoyek
article en

Abstract

The objective of this study is to investigate the oxide removal and the reoxidation mechanisms occurring on indium phosphide (InP) surfaces in a cleanroom environment after HCl wet treatments. For this purpose, an experimental setup was mounted, tuned and validated consisting of a glove box connected to a X-ray photoelectron spectroscopy (XPS) chamber, enabling quasi in-situ sample transfer after HCl wet treatment without any air exposure. We showed that a dip of at least 3 min in HCl with a concentration of at least 0.5% (0.137 mol/L) effectively removed indium phosphates (InPO x ) from InP surfaces. Reoxidation of HCl-treated InP surfaces was observed after more than 1 min of air exposure.

Diffusion and defect data, solid state data. Part B, Solid state phenomena/Solid state phenomenaVol. 395
Centre National de la Recherche Scientifique (FR), Commissariat à l'Énergie Atomique et aux Énergies Alternatives (FR), Laboratoire d'Électronique des Technologies de l'Information (FR), Université Grenoble Alpes (FR)
Openalex Percentile: Top 24%
Semiconductor materials and devices
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