Inulin–Calendula officinalis Dermatocosmetic Hydrogels: Development, Physicochemical Characterization and Texture Profile Analysis

This study investigated dermatocosmetic hydrogel formulations containing inulin and a quality-controlled organic Calendula officinalis L. flower extract in 20% propylene glycol, with emphasis on physicochemical and textural characterization. Seven formulations were prepared and evaluated for organoleptic characteristics, pH, firmness, cohesiveness, springiness, and resilience. All formulations were macroscopically homogeneous, while pH values ranged from 6.28 ± 0.01 to 6.66 ± 0.04. Texture Profile Analysis revealed formulation-dependent mechanical behaviour. Firmness ranged from 0.430 ± 0.002 to 0.698 ± 0.042 N, cohesiveness from 0.660 ± 0.009 to 0.874 ± 0.013, springiness from 0.778 ± 0.001 to 0.941 ± 0.037, and resilience from 0.277 ± 0.005 to 0.494 ± 0.016. One-way ANOVA indicated an overall formulation effect for all four texture parameters (p < 0.0001), followed by Tukey HSD pairwise comparisons. Gel 2, containing 2% inulin without Calendula officinalis extract, exhibited the highest numerical firmness and springiness, whereas Gel 5, containing 4% inulin and 3% Calendula officinalis extract, showed the highest cohesiveness and resilience. The extract-only Gel 6 displayed the lowest numerical values for all four texture parameters. The results support a formulation-dependent, non-linear effect of inulin on gel mechanical behaviour and provide a physicochemical basis for subsequent rheological, stability, phytochemical, release, safety, and biological investigations.

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Publication Details

Journal
Gels
Published
2026-10-27
DOI
https://doi.org/10.3390/gels12110977
Primary Topic
Hydrogels: synthesis, properties, applications
Type
article
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article

Inulin–Calendula officinalis Dermatocosmetic Hydrogels: Development, Physicochemical Characterization and Texture Profile Analysis

Fawzia Sha’at, Mihaela Carmen Eremia, Anca Daniela Raiciu, Ramona‐Daniela Pavaloiu et al.
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Gels
Hydrogels: synthesis, properties, applications
article

Inulin–Calendula officinalis Dermatocosmetic Hydrogels: Development, Physicochemical Characterization and Texture Profile Analysis

Fawzia Sha’at, Mihaela Carmen Eremia, Anca Daniela Raiciu, Ramona‐Daniela Pavaloiu, Amalia Ștefaniu
article en

Abstract

This study investigated dermatocosmetic hydrogel formulations containing inulin and a quality-controlled organic Calendula officinalis L. flower extract in 20% propylene glycol, with emphasis on physicochemical and textural characterization. Seven formulations were prepared and evaluated for organoleptic characteristics, pH, firmness, cohesiveness, springiness, and resilience. All formulations were macroscopically homogeneous, while pH values ranged from 6.28 ± 0.01 to 6.66 ± 0.04. Texture Profile Analysis revealed formulation-dependent mechanical behaviour. Firmness ranged from 0.430 ± 0.002 to 0.698 ± 0.042 N, cohesiveness from 0.660 ± 0.009 to 0.874 ± 0.013, springiness from 0.778 ± 0.001 to 0.941 ± 0.037, and resilience from 0.277 ± 0.005 to 0.494 ± 0.016. One-way ANOVA indicated an overall formulation effect for all four texture parameters (p < 0.0001), followed by Tukey HSD pairwise comparisons. Gel 2, containing 2% inulin without Calendula officinalis extract, exhibited the highest numerical firmness and springiness, whereas Gel 5, containing 4% inulin and 3% Calendula officinalis extract, showed the highest cohesiveness and resilience. The extract-only Gel 6 displayed the lowest numerical values for all four texture parameters. The results support a formulation-dependent, non-linear effect of inulin on gel mechanical behaviour and provide a physicochemical basis for subsequent rheological, stability, phytochemical, release, safety, and biological investigations.

GelsVol. 12(11)
Titu Maiorescu University (RO), National Institute For Chemical Pharmaceutical Research and Development (RO)
Openalex Percentile: Top 22%
Hydrogels: synthesis, properties, applications
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Inulin–Calendula officinalis Dermatocosmetic Hydrogels: Development, Physicochemical Characterization and Texture Profile Analysis — Fawzia Sha’at, Mihaela Carmen Eremia, et al. · Gels (2026) | TGRS Research Map | TGRS