Repair of direct restorative materials with a self-adhesive composite hybrid: Effects of substrate, surface pretreatment, and aging

Objectives To evaluate the effects of restorative substrate, pre-repair substrate aging, airborne-particle abrasion, adhesive application, and post-repair aging on the shear bond strength (SBS) of repairs performed with a self-adhesive composite hybrid. Methods The substrates were a conventional glass-ionomer cement (ChemFil Rock), a nanohybrid resin composite (Ceram.x Spectra ST), and a composite hybrid (Surefil one), which also served as the repair material in all groups. A 3 × 2 × 2 × 2 × 2 factorial design comprised 48 groups (n = 9; total n = 432). Substrates were thermocycled or unaged, standardized by P320 grinding, and optionally subjected to airborne-particle abrasion with 50-μm Al 2 O 3 and/or adhesive application. Completed repairs were thermocycled or left unaged. SBS was analyzed using a categorical fixed-effects model with HC3-robust inference and planned Welch comparisons with Holm adjustment. Pre-test failures (PTFs) were included as 0 MPa. Results Sixty-eight PTFs occurred (15.7%): 51 with the glass-ionomer cement, 17 with the composite hybrid, and none with the conventional composite. Significant main effects were found for all five experimental factors (p < 0.001). Under dual aging, the complete pretreatment protocol yielded the highest mean SBS for every substrate: 2.75 MPa for the glass-ionomer cement, 11.65 MPa for the conventional composite, and 12.60 MPa for the composite hybrid. Significance Surefil one showed potential for repairing the tested aged resin-containing substrates when the tested external adhesive was applied, whereas bonding to ChemFil Rock remained weak after aging. The substrate-dependent response highlights the importance of material composition in repair-protocol selection.

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Publication Details

Journal
International Journal of Adhesion and Adhesives
Published
2026-10-03
DOI
https://doi.org/10.1016/j.ijadhadh.2026.104502
Primary Topic
Dental materials and restorations
Type
article
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article

Repair of direct restorative materials with a self-adhesive composite hybrid: Effects of substrate, surface pretreatment, and aging

Dominik Kraus, Helmut Stark, Michael Marder, Milan Stoilov et al.
International Journal of Adhesion and Adhesives
Dental materials and restorations
article

Repair of direct restorative materials with a self-adhesive composite hybrid: Effects of substrate, surface pretreatment, and aging

Dominik Kraus, Helmut Stark, Michael Marder, Milan Stoilov, Norbert Enkling, Marvin Amann
article en

Abstract

Objectives To evaluate the effects of restorative substrate, pre-repair substrate aging, airborne-particle abrasion, adhesive application, and post-repair aging on the shear bond strength (SBS) of repairs performed with a self-adhesive composite hybrid. Methods The substrates were a conventional glass-ionomer cement (ChemFil Rock), a nanohybrid resin composite (Ceram.x Spectra ST), and a composite hybrid (Surefil one), which also served as the repair material in all groups. A 3 × 2 × 2 × 2 × 2 factorial design comprised 48 groups (n = 9; total n = 432). Substrates were thermocycled or unaged, standardized by P320 grinding, and optionally subjected to airborne-particle abrasion with 50-μm Al 2 O 3 and/or adhesive application. Completed repairs were thermocycled or left unaged. SBS was analyzed using a categorical fixed-effects model with HC3-robust inference and planned Welch comparisons with Holm adjustment. Pre-test failures (PTFs) were included as 0 MPa. Results Sixty-eight PTFs occurred (15.7%): 51 with the glass-ionomer cement, 17 with the composite hybrid, and none with the conventional composite. Significant main effects were found for all five experimental factors (p < 0.001). Under dual aging, the complete pretreatment protocol yielded the highest mean SBS for every substrate: 2.75 MPa for the glass-ionomer cement, 11.65 MPa for the conventional composite, and 12.60 MPa for the composite hybrid. Significance Surefil one showed potential for repairing the tested aged resin-containing substrates when the tested external adhesive was applied, whereas bonding to ChemFil Rock remained weak after aging. The substrate-dependent response highlights the importance of material composition in repair-protocol selection.

International Journal of Adhesion and AdhesivesVol. 153
University of Bern (CH), University of Bonn (DE)
Openalex Percentile: Top 9%
Dental materials and restorations
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