Prediction of gradient microstructure distribution of grinding metamorphic layer in 8Cr4Mo4V steel by colourful oxide films

Grinding-induced thermal loads can alter the near-surface microstructure of hardened bearing steels. This study proposes a semi-quantitative post-process method for associating oxide-film interference colour with the grinding-induced metamorphic layer in 8Cr4Mo4V steel. Furnace specimens were oxidized for 30 s at 200°C–400°C under fixed imaging conditions. Oxide colour was recorded by CCD imaging, optical-equivalent film thickness was estimated using thin-film interference theory, and EDS was used to compare oxygen-enrichment trends. Grinding tests were conducted at depths of cut of 6, 12, 18 and 24 μ m, followed by cross-sectional CCD and FESEM observations and finite-element temperature analysis. The furnace colour changed from pale yellow to blue-grey, with calculated optical-equivalent thicknesses of approximately 125–605 nm. Increasing the grinding depth from 6 to 24 μ m increased the simulated peak surface temperature from approximately 450°C to 760°C and the observed colour-zone depth from approximately 7 to 23 μ m. The deeper colour zones were associated with a transition from predominantly acicular tempered martensite to a cryptocrystalline-martensite-dominated region and a mixed transition zone. A descriptive comparison gave R 2 = 0 . 997 . Because neither physical film thickness nor grinding temperature was measured directly, the proposed relationship represents quantitative trend consistency rather than direct validation. The method is intended for low-cost post-process screening rather than absolute temperature, film-thickness or phase-fraction measurement.

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Publication Details

Journal
Proceedings of the Institution of Mechanical Engineers Part B Journal of Engineering Manufacture
Published
2026-09-30
DOI
https://doi.org/10.1177/09544054261492512
Primary Topic
Advanced machining processes and optimization
Type
article
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article

Prediction of gradient microstructure distribution of grinding metamorphic layer in 8Cr4Mo4V steel by colourful oxide films

Jiaxu Guo, Haitao Liu, BoHan Zhang, Yuhan Wang et al.
Proceedings of the Institution of Mechanical Engineers Part B Journal of Engineering Manufacture
Advanced machining processes and optimization
article

Prediction of gradient microstructure distribution of grinding metamorphic layer in 8Cr4Mo4V steel by colourful oxide films

Jiaxu Guo, Haitao Liu, BoHan Zhang, Yuhan Wang, Yazhou Sun, Hangqi Zhang, Xubo Fan
article en

Abstract

Grinding-induced thermal loads can alter the near-surface microstructure of hardened bearing steels. This study proposes a semi-quantitative post-process method for associating oxide-film interference colour with the grinding-induced metamorphic layer in 8Cr4Mo4V steel. Furnace specimens were oxidized for 30 s at 200°C–400°C under fixed imaging conditions. Oxide colour was recorded by CCD imaging, optical-equivalent film thickness was estimated using thin-film interference theory, and EDS was used to compare oxygen-enrichment trends. Grinding tests were conducted at depths of cut of 6, 12, 18 and 24 μ m, followed by cross-sectional CCD and FESEM observations and finite-element temperature analysis. The furnace colour changed from pale yellow to blue-grey, with calculated optical-equivalent thicknesses of approximately 125–605 nm. Increasing the grinding depth from 6 to 24 μ m increased the simulated peak surface temperature from approximately 450°C to 760°C and the observed colour-zone depth from approximately 7 to 23 μ m. The deeper colour zones were associated with a transition from predominantly acicular tempered martensite to a cryptocrystalline-martensite-dominated region and a mixed transition zone. A descriptive comparison gave R 2 = 0 . 997 . Because neither physical film thickness nor grinding temperature was measured directly, the proposed relationship represents quantitative trend consistency rather than direct validation. The method is intended for low-cost post-process screening rather than absolute temperature, film-thickness or phase-fraction measurement.

Proceedings of the Institution of Mechanical Engineers Part B Journal of Engineering Manufacture
Heilongjiang Institute of Technology (CN)
Openalex Percentile: Top 21%
Advanced machining processes and optimization
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Prediction of gradient microstructure distribution of grinding metamorphic layer in 8Cr4Mo4V steel by colourful oxide films — Jiaxu Guo, Haitao Liu, et al. · Proceedings of the Institution of Mechanical Engineers Part B Journal of Engineering Manufacture (2026) | TGRS Research Map | TGRS