Synergistic Valorization of Ternary Industrial Solid Wastes for Sustainable Loess Stabilization: Mix Optimization, Strength Evolution, and Microstructural Mechanisms

This study investigates the mechanical properties and strength formation mechanism of loess solidified with a ternary blend of fly ash, lithium slag, and magnesium slag. The mix proportion was optimized using response surface methodology with a Box–Behnken design. Unconfined compressive strength (UCS) tests, digital image correlation (DIC), X-ray diffraction (XRD), and scanning electron microscopy (SEM) were employed for evaluation. The optimal 7-day mix (15.926 wt.% fly ash, 10.158 wt.% lithium slag, and 6.427 wt.% magnesium slag) achieved a UCS of 0.974 MPa, while the 28-day optimum (16.064 wt.% fly ash, 10 wt.% lithium slag, and 2 wt.% magnesium slag) yielded 1.834 MPa. Strength development followed a quadratic nonlinear model at early age, shifting to a linear superposition model at 28 days. XRD and SEM revealed that strength enhancement originates from synergistic pozzolanic and hydration reactions under alkaline activation, producing C-S-H gel and ettringite (AFt) that fill pores and cement soil particles. The ternary system demonstrates effective utilization of industrial solid wastes for loess stabilization.

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Journal
Materials
Published
2026-09-20
DOI
https://doi.org/10.3390/ma19183999
Primary Topic
Concrete and Cement Materials Research
Type
article
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Synergistic Valorization of Ternary Industrial Solid Wastes for Sustainable Loess Stabilization: Mix Optimization, Strength Evolution, and Microstructural Mechanisms

Bowen Guan, Anhua Xu, Jing Li, Yuanji Li et al.
Materials
Concrete and Cement Materials Research
article

Synergistic Valorization of Ternary Industrial Solid Wastes for Sustainable Loess Stabilization: Mix Optimization, Strength Evolution, and Microstructural Mechanisms

Bowen Guan, Anhua Xu, Jing Li, Yuanji Li, Yindong Xu, Yushu Jing, Yonghai Gu
article en

Abstract

This study investigates the mechanical properties and strength formation mechanism of loess solidified with a ternary blend of fly ash, lithium slag, and magnesium slag. The mix proportion was optimized using response surface methodology with a Box–Behnken design. Unconfined compressive strength (UCS) tests, digital image correlation (DIC), X-ray diffraction (XRD), and scanning electron microscopy (SEM) were employed for evaluation. The optimal 7-day mix (15.926 wt.% fly ash, 10.158 wt.% lithium slag, and 6.427 wt.% magnesium slag) achieved a UCS of 0.974 MPa, while the 28-day optimum (16.064 wt.% fly ash, 10 wt.% lithium slag, and 2 wt.% magnesium slag) yielded 1.834 MPa. Strength development followed a quadratic nonlinear model at early age, shifting to a linear superposition model at 28 days. XRD and SEM revealed that strength enhancement originates from synergistic pozzolanic and hydration reactions under alkaline activation, producing C-S-H gel and ettringite (AFt) that fill pores and cement soil particles. The ternary system demonstrates effective utilization of industrial solid wastes for loess stabilization.

MaterialsVol. 19(18)
Qinghai University (CN), Chang'an University (CN), Qinghai Tibetan Hospital (CN)
Industry, innovation and infrastructure
Openalex Percentile: Top 17%
Concrete and Cement Materials Research
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Synergistic Valorization of Ternary Industrial Solid Wastes for Sustainable Loess Stabilization: Mix Optimization, Strength Evolution, and Microstructural Mechanisms — Bowen Guan, Anhua Xu, et al. · Materials (2026) | TGRS Research Map | TGRS