Reductive C–O Bond Cleavage and Borylation of Carboxylic Esters

Abstract Alcohols are abundant feedstocks in organic synthesis but remain underutilized as alkyl donors via C–O bond activation. In this work, the deoxygenative Markó–Lam reaction is studied computationally to probe how the reductive radical transformation may be tuned to efficiently furnish open-shell intermediates. The theoretical results were experimentally illustrated for deoxyborylation of a series of benzylic esters.

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Publication Details

Journal
ACS electrochemistry.
Published
2026-09-18
DOI
https://doi.org/10.1021/acselectrochem.6c00123
Primary Topic
Organoboron and organosilicon chemistry
Type
article
Field-Weighted Citation Impact
0.00

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article

Reductive C–O Bond Cleavage and Borylation of Carboxylic Esters

Helena Lundberg, Mårten S. G. Ahlquist, Julius Kuzmin, Julia Rune et al.
ACS electrochemistry.
Organoboron and organosilicon chemistry
article

Reductive C–O Bond Cleavage and Borylation of Carboxylic Esters

Helena Lundberg, Mårten S. G. Ahlquist, Julius Kuzmin, Julia Rune, Alexandros Xanthopoulos
article en

Abstract

Abstract Alcohols are abundant feedstocks in organic synthesis but remain underutilized as alkyl donors via C–O bond activation. In this work, the deoxygenative Markó–Lam reaction is studied computationally to probe how the reductive radical transformation may be tuned to efficiently furnish open-shell intermediates. The theoretical results were experimentally illustrated for deoxyborylation of a series of benzylic esters.

ACS electrochemistry.
KTH Royal Institute of Technology (SE)
Kungliga Tekniska Högskolan, Vetenskapsrådet, Stiftelsen för Strategisk Forskning, European Research Council
Openalex Percentile: Top 21%
Organoboron and organosilicon chemistry
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