Influence of carbonate apatite nanoparticles incorporated into commercial dental adhesives on immediate and long‐term microtensile bond strength

molar ratio of 5 (CA5n) into commercial adhesives affected the immediate or the long-term microtensile bond strength (µTBS) between composite resin and dentin. Scotchbond Multipurpose and Scotchbond Universal were tested with 0, 0.5, and 1 wt.% CA5n added. For Multipurpose, CA5n were incorporated into either the primer or the adhesive. Solutions were sonicated to minimize agglomeration. Sound human molars (n = 6/group) were prepared, and modified adhesives were applied as instructed. Composite was incrementally built up to 4 mm thick. Specimens were sectioned into beams and stored in water for 24 h or for 6 months before testing. Failure modes were observed. Data were analyzed using aligned rank transform anova (α < 0.05). CA5n had no impact on the bond strength of Multipurpose at either time point, irrespective of placement. Universal with 1% CA5n exhibited significantly higher 24 h µTBS than all other groups, but this advantage declined after 6 months. Mixed and adhesive failures increased over time, with the highest adhesive failure in Universal 1% at 6 months. Incorporation of CA5n into the tested adhesive systems did not significantly affect µTBS at 24 h or after 6 months of aging.

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Publication Details

Journal
European Journal Of Oral Sciences
Published
2026-09-17
DOI
https://doi.org/10.1111/eos.70138
Primary Topic
Dental materials and restorations
Type
article
Field-Weighted Citation Impact
0.00

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article

Influence of carbonate apatite nanoparticles incorporated into commercial dental adhesives on immediate and long‐term microtensile bond strength

Jon E. Dahl, Mina Aker Sagen, Heba E. AbdelRazik
European Journal Of Oral Sciences
Dental materials and restorations
article

Influence of carbonate apatite nanoparticles incorporated into commercial dental adhesives on immediate and long‐term microtensile bond strength

Jon E. Dahl, Mina Aker Sagen, Heba E. AbdelRazik
article en

Abstract

molar ratio of 5 (CA5n) into commercial adhesives affected the immediate or the long-term microtensile bond strength (µTBS) between composite resin and dentin. Scotchbond Multipurpose and Scotchbond Universal were tested with 0, 0.5, and 1 wt.% CA5n added. For Multipurpose, CA5n were incorporated into either the primer or the adhesive. Solutions were sonicated to minimize agglomeration. Sound human molars (n = 6/group) were prepared, and modified adhesives were applied as instructed. Composite was incrementally built up to 4 mm thick. Specimens were sectioned into beams and stored in water for 24 h or for 6 months before testing. Failure modes were observed. Data were analyzed using aligned rank transform anova (α < 0.05). CA5n had no impact on the bond strength of Multipurpose at either time point, irrespective of placement. Universal with 1% CA5n exhibited significantly higher 24 h µTBS than all other groups, but this advantage declined after 6 months. Mixed and adhesive failures increased over time, with the highest adhesive failure in Universal 1% at 6 months. Incorporation of CA5n into the tested adhesive systems did not significantly affect µTBS at 24 h or after 6 months of aging.

European Journal Of Oral Sciences
University of Turku (FI), Nordic Institute of Dental Materials (NO), Turku University Hospital (FI)
Instytut Medycyny Pracy im. prof. J. Nofera, Nordic Institute of Dental Materials
Clean water and sanitation
Openalex Percentile: Top 9%
Dental materials and restorations
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Influence of carbonate apatite nanoparticles incorporated into commercial dental adhesives on immediate and long‐term microtensile bond strength — Jon E. Dahl, Mina Aker Sagen, et al. · European Journal Of Oral Sciences (2026) | TGRS Research Map | TGRS