Practical Guide to Analyzing Dynamics Using X-ray Photon Correlation Spectroscopy (XPCS)

X-ray photon correlation spectroscopy (XPCS) provides access to nanoscale dynamics, yet practical approaches for interpreting its data remain limited. This tutorial presents a systematic framework for XPCS data analysis, illustrated using measurements performed at the NSLS-II CHX beamline. The fundamental concepts of speckle pattern and the intensity autocorrelation function are introduced, followed by ferroelectric case studies demonstrating how polarization switching and phase transition dynamics can be extracted from XPCS measurements. The influence of the probed q-range experimental conditions such as X-ray transmittance is examined for data interpretation. These elements are consolidated into practical guidelines for the reliable analysis of XPCS data.

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Publication Details

Journal
Journal of the Korean Institute of Electrical and Electronic Material Engineers
Published
2026-09-01
DOI
https://doi.org/10.4313/jeem.2026.39.5.3
Primary Topic
Material Dynamics and Properties
Type
article
Field-Weighted Citation Impact
0.00

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article

Practical Guide to Analyzing Dynamics Using X-ray Photon Correlation Spectroscopy (XPCS)

Jong Eun Ryu, Wook Jo, Jeong‐Woo Sun
Journal of the Korean Institute of Electrical and Electronic Material Engineers
Material Dynamics and Properties
article

Practical Guide to Analyzing Dynamics Using X-ray Photon Correlation Spectroscopy (XPCS)

Jong Eun Ryu, Wook Jo, Jeong‐Woo Sun
article en

Abstract

X-ray photon correlation spectroscopy (XPCS) provides access to nanoscale dynamics, yet practical approaches for interpreting its data remain limited. This tutorial presents a systematic framework for XPCS data analysis, illustrated using measurements performed at the NSLS-II CHX beamline. The fundamental concepts of speckle pattern and the intensity autocorrelation function are introduced, followed by ferroelectric case studies demonstrating how polarization switching and phase transition dynamics can be extracted from XPCS measurements. The influence of the probed q-range experimental conditions such as X-ray transmittance is examined for data interpretation. These elements are consolidated into practical guidelines for the reliable analysis of XPCS data.

Journal of the Korean Institute of Electrical and Electronic Material EngineersVol. 39(5)
Georgia Institute of Technology (US), North Carolina State University (US), Ulsan National Institute of Science and Technology (KR)
U.S. Department of Energy, Korea Electrotechnology Research Institute, Ministry of Science and ICT, South Korea, Office of Science, Brookhaven National Laboratory
Openalex Percentile: Top 24%
Material Dynamics and Properties
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