Turmeric essential oil‐loaded wheat starch cryogels as superabsorbent pads for active packaging of fish fillets

BACKGROUND: This study aimed to create a cryogel with water-absorbing and antioxidant properties. Wheat starch (10%, w/v) was used to produce cryogels, which were then incorporated with turmeric essential oil (TEO) at two concentrations: 20% and 30% (w/w of starch). The production method consisted of gelatinization, freeze/thaw cycles, and subsequent freeze-drying. The materials were applied as an absorbent pad for fish fillet exudate. The major compounds of TEO were ar-turmerone (43.60%) and α-turmerone (23.49%), characterized by gas chromatography. RESULTS: ) and high porosity (85.97%), not differing among the formulations. The water absorption capacity was high, with the control (0% TEO) reaching 1026% and reducing for those with TEO to approximately 883%. Cryogels demonstrated a high TEO loading capacity, exceeding 90%. In vitro release showed that, after 2880 min, the 30% TEO cryogels released 22% of their content in a hydrophilic medium and a substantially higher 69% in a lipophilic medium. The cryogels with 30% TEO achieved an antioxidant activity of 48% for ABTS [i.e. 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid)] radical inhibition and 23% for DPPH (i.e. 2,2-diphenyl-1-picrylhydrazyl) radical. When applied to fish fillets, after 7 days of storage, the cryogels maintained stable pH (6.06) and mass loss (5.6%) across treatments, at the same time as showing a comparable exudate absorption of approximately 35%. CONCLUSION: Exhibiting water-absorbing capacity, high loading capacity, controlled in vitro release, and antioxidant activity. The developed materials are promising three-dimensional materials for active food packaging applications in fish fillet preservation. © 2026 The Author(s). Journal of the Science of Food and Agriculture published by John Wiley & Sons Ltd on behalf of Society of Chemical Industry.

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Journal
Journal of the Science of Food and Agriculture
Published
2026-06-17
DOI
https://doi.org/10.1002/jsfa.70764
Primary Topic
Nanocomposite Films for Food Packaging
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article
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article

Turmeric essential oil‐loaded wheat starch cryogels as superabsorbent pads for active packaging of fish fillets

Camila de Oliveira Pacheco, Élder Pacheco da Cruz, Laura Martins Fonseca, Elessandra da Rosa Zavareze et al.
Journal of the Science of Food and Agriculture
Nanocomposite Films for Food Packaging
article

Turmeric essential oil‐loaded wheat starch cryogels as superabsorbent pads for active packaging of fish fillets

Camila de Oliveira Pacheco, Élder Pacheco da Cruz, Laura Martins Fonseca, Elessandra da Rosa Zavareze, Gabriel Lucas Pail, Cristina Jansen, Rosane Lopes Crizel, Alvaro Renato Guerra Dias
article en

Abstract

BACKGROUND: This study aimed to create a cryogel with water-absorbing and antioxidant properties. Wheat starch (10%, w/v) was used to produce cryogels, which were then incorporated with turmeric essential oil (TEO) at two concentrations: 20% and 30% (w/w of starch). The production method consisted of gelatinization, freeze/thaw cycles, and subsequent freeze-drying. The materials were applied as an absorbent pad for fish fillet exudate. The major compounds of TEO were ar-turmerone (43.60%) and α-turmerone (23.49%), characterized by gas chromatography. RESULTS: ) and high porosity (85.97%), not differing among the formulations. The water absorption capacity was high, with the control (0% TEO) reaching 1026% and reducing for those with TEO to approximately 883%. Cryogels demonstrated a high TEO loading capacity, exceeding 90%. In vitro release showed that, after 2880 min, the 30% TEO cryogels released 22% of their content in a hydrophilic medium and a substantially higher 69% in a lipophilic medium. The cryogels with 30% TEO achieved an antioxidant activity of 48% for ABTS [i.e. 2,2'-azino-bis(3-ethylbenzothiazoline-6-sulfonic acid)] radical inhibition and 23% for DPPH (i.e. 2,2-diphenyl-1-picrylhydrazyl) radical. When applied to fish fillets, after 7 days of storage, the cryogels maintained stable pH (6.06) and mass loss (5.6%) across treatments, at the same time as showing a comparable exudate absorption of approximately 35%. CONCLUSION: Exhibiting water-absorbing capacity, high loading capacity, controlled in vitro release, and antioxidant activity. The developed materials are promising three-dimensional materials for active food packaging applications in fish fillet preservation. © 2026 The Author(s). Journal of the Science of Food and Agriculture published by John Wiley & Sons Ltd on behalf of Society of Chemical Industry.

Journal of the Science of Food and Agriculture
Universidade Federal de Pelotas (BR)
Openalex Percentile: Top 12%
Nanocomposite Films for Food Packaging
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