Blue-light DLP of high-performance dental 3YSZ ceramics: optimized sintering, mechanical reliability and biocompatibility

Purpose Additive manufacturing of zirconia dental restorations remains constrained by insufficient densification, mechanical properties and dimensional stability compared with computer-aided design and computer-aided manufacturing (CAD/CAM) processing. This study aims to establish a blue-light digital light processing (DLP) route for fabricating high-solid-loading 3 mol% yttria-stabilized zirconia (3YSZ) ceramics and to evaluate its suitability for high-performance dental applications. Design/methodology/approach High-solid-loading (58 Vol.%) 3YSZ slurries were processed using blue-light (465 nm) DLP stereolithography and pressureless sintering at 1400°C–1500°C. The effects of sintering temperature on densification behavior, microstructural evolution, mechanical properties, wear resistance and cytocompatibility were systematically investigated using density measurements, SEM, mechanical testing, tribological analysis and in-vitro cell viability assays. Findings Near-theoretical densities (5.92–5.95 g/cm3) with low porosity (0.16%–0.23%) and uniform linear shrinkage below 20% were achieved, indicating excellent dimensional stability. Optimized sintering at 1500°C produced fine-grained, highly densified microstructures with improved interlayer cohesion. The resulting ceramics exhibited a flexural strength of 799.34 ± 58.51 MPa in horizontal plane orientation and 625.96 ± 34.10 MPa in vertical plane orientation, a hardness of 13.66 ± 0.11 GPa and an elastic modulus of 109.50 ± 0.89 GPa, approaching those of conventionally manufactured zirconia. The flexural strength ratio σv/σh was 0.78, demonstrating low mechanical anisotropy. Wear resistance and cytocompatibility were comparable to clinical-grade zirconia ceramics. Originality/value This study proposes and validates a fabrication route combining an optimized high-solid-loading slurry formulation with blue-light DLP, overcoming the key limitations of UV-based stereolithography in processing high-solid-loading 3YSZ slurries and producing 3YSZ ceramics whose mechanical properties and dimensional stability approach those of CAD/CAM-manufactured counterparts. The authors systematically characterized the mechanical, tribological and biological properties of the resulting 3YSZ ceramics, providing critical data to support blue-light DLP as a viable manufacturing route for high-performance personalized dental restorations.

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Publication Details

Journal
Rapid Prototyping Journal
Published
2026-06-18
DOI
https://doi.org/10.1108/rpj-02-2026-0104
Primary Topic
Dental materials and restorations
Type
article
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article

Blue-light DLP of high-performance dental 3YSZ ceramics: optimized sintering, mechanical reliability and biocompatibility

Zhongkan Ren, Rui Xing, Z Y Liu, Zhuhui Qiao
Rapid Prototyping Journal
Dental materials and restorations
article

Blue-light DLP of high-performance dental 3YSZ ceramics: optimized sintering, mechanical reliability and biocompatibility

Zhongkan Ren, Rui Xing, Z Y Liu, Zhuhui Qiao
article en

Abstract

Purpose Additive manufacturing of zirconia dental restorations remains constrained by insufficient densification, mechanical properties and dimensional stability compared with computer-aided design and computer-aided manufacturing (CAD/CAM) processing. This study aims to establish a blue-light digital light processing (DLP) route for fabricating high-solid-loading 3 mol% yttria-stabilized zirconia (3YSZ) ceramics and to evaluate its suitability for high-performance dental applications. Design/methodology/approach High-solid-loading (58 Vol.%) 3YSZ slurries were processed using blue-light (465 nm) DLP stereolithography and pressureless sintering at 1400°C–1500°C. The effects of sintering temperature on densification behavior, microstructural evolution, mechanical properties, wear resistance and cytocompatibility were systematically investigated using density measurements, SEM, mechanical testing, tribological analysis and in-vitro cell viability assays. Findings Near-theoretical densities (5.92–5.95 g/cm3) with low porosity (0.16%–0.23%) and uniform linear shrinkage below 20% were achieved, indicating excellent dimensional stability. Optimized sintering at 1500°C produced fine-grained, highly densified microstructures with improved interlayer cohesion. The resulting ceramics exhibited a flexural strength of 799.34 ± 58.51 MPa in horizontal plane orientation and 625.96 ± 34.10 MPa in vertical plane orientation, a hardness of 13.66 ± 0.11 GPa and an elastic modulus of 109.50 ± 0.89 GPa, approaching those of conventionally manufactured zirconia. The flexural strength ratio σv/σh was 0.78, demonstrating low mechanical anisotropy. Wear resistance and cytocompatibility were comparable to clinical-grade zirconia ceramics. Originality/value This study proposes and validates a fabrication route combining an optimized high-solid-loading slurry formulation with blue-light DLP, overcoming the key limitations of UV-based stereolithography in processing high-solid-loading 3YSZ slurries and producing 3YSZ ceramics whose mechanical properties and dimensional stability approach those of CAD/CAM-manufactured counterparts. The authors systematically characterized the mechanical, tribological and biological properties of the resulting 3YSZ ceramics, providing critical data to support blue-light DLP as a viable manufacturing route for high-performance personalized dental restorations.

Rapid Prototyping Journal
Binzhou Medical University (CN), Shandong University of Aeronautics (CN), Yantai University (CN), Lanzhou Institute of Chemical Physics (CN), Yantai Institute of Coastal Zone Research (CN)
Openalex Percentile: Top 6%
Dental materials and restorations
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