Potential of VIS‐IR imaging spectroscopy and SEM‐EDS and EMPA to map the mineralogical composition of NWA 7317 (CR6)

Abstract Asteroid compositional analysis relies on comparing reflectance spectra with laboratory data from well‐characterized meteorites. To advance this comparison, we performed a comprehensive laboratory analysis on a slab of the Northwest Africa (NWA) 7317—CR6 carbonaceous chondrite. We employed high‐resolution Visible‐Infrared (VIS‐IR) imaging spectroscopy (0.4–5.1 μm) using the SPIM hyperspectral facility, integrated with high‐spatial‐resolution elemental mapping via SEM‐EDS and EMPA‐WDS. This multi‐technique approach enabled the retrieval of surface composition at high spectral and spatial resolutions. Our results, supported by ICA/PCA and K‐means classification methodologies, highlight the challenges of integrating VIS‐IR spectroscopy and SEM/EMPA at the micrometer scale. While both techniques consistently infer an overall poikiloblastic/metamorphic texture dominated by an olivine and pyroxene‐rich matrix, their combined use requires a critical approach for robust analysis. The absence of the 3 μm absorption band indicates high temperatures during thermal metamorphism on the NWA 7317 parent body. Although FeNi metallic alloys and Fe‐sulfide inclusions contribute to the VIS‐IR spectroscopic signal, they are not clearly distinguishable from each other. Furthermore, minor phases like plagioclase and chromite detected via SEM/EMPA are not plainly visible in the SPIM results. We review the potential of integrating these techniques to assess the petrography, mineralogy, and terrestrial weathering of NWA 7317.

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Publication Details

Journal
Meteoritics and Planetary Science
Published
2026-05-14
DOI
https://doi.org/10.1111/maps.70170
Primary Topic
Astro and Planetary Science
Type
article
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Potential of VIS‐IR imaging spectroscopy and SEM‐EDS and EMPA to map the mineralogical composition of NWA 7317 (CR6)

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article

Potential of VIS‐IR imaging spectroscopy and SEM‐EDS and EMPA to map the mineralogical composition of NWA 7317 (CR6)

Antonio Lettino, Angelo Palombo, Anna Galiano, Giovanni Pratesi, Simone Pascucci, Gianrico Filacchione, Simone De Angelis, Tiberio Cuppone, Maria Cristina De Sanctis, Eliana La Francesca, Martina Casalini
article en

Abstract

Abstract Asteroid compositional analysis relies on comparing reflectance spectra with laboratory data from well‐characterized meteorites. To advance this comparison, we performed a comprehensive laboratory analysis on a slab of the Northwest Africa (NWA) 7317—CR6 carbonaceous chondrite. We employed high‐resolution Visible‐Infrared (VIS‐IR) imaging spectroscopy (0.4–5.1 μm) using the SPIM hyperspectral facility, integrated with high‐spatial‐resolution elemental mapping via SEM‐EDS and EMPA‐WDS. This multi‐technique approach enabled the retrieval of surface composition at high spectral and spatial resolutions. Our results, supported by ICA/PCA and K‐means classification methodologies, highlight the challenges of integrating VIS‐IR spectroscopy and SEM/EMPA at the micrometer scale. While both techniques consistently infer an overall poikiloblastic/metamorphic texture dominated by an olivine and pyroxene‐rich matrix, their combined use requires a critical approach for robust analysis. The absence of the 3 μm absorption band indicates high temperatures during thermal metamorphism on the NWA 7317 parent body. Although FeNi metallic alloys and Fe‐sulfide inclusions contribute to the VIS‐IR spectroscopic signal, they are not clearly distinguishable from each other. Furthermore, minor phases like plagioclase and chromite detected via SEM/EMPA are not plainly visible in the SPIM results. We review the potential of integrating these techniques to assess the petrography, mineralogy, and terrestrial weathering of NWA 7317.

Meteoritics and Planetary Science
Institute for Space Astrophysics and Planetology (IT), CNR-IMIOT – Consiglio Nazionale delle Ricerche - Istituto di Metodologie Integrate per l’Osservazione della Terra (IT), University of Florence (IT)
Openalex Percentile: Top 4%
Astro and Planetary Science
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