Data Acquisition System for the Tender-Energy Spectroscopy Beamline at the Shanghai Synchrotron Radiation Facility

A dedicated data acquisition system has been developed and commissioned for the tender-energy spectroscopy beamline BL16U1 at the Shanghai Synchrotron Radiation Facility. The system implements a distributed architecture integrating EPICS-based hardware control with the Bluesky experiment orchestration environment, supporting multiple X-ray absorption spectroscopy modes including transmission, total electron yield, total fluorescence yield, and partial fluorescence yield detection. A key technical feature is the hardware-level synchronization between a multi-channel silicon drift detector and a multichannel scaler, enabling precise timing for fluorescence-XAS measurements. A unified graphical interface based on Control System Studio provides streamlined experiment control and real-time data visualization. System validation using standard reference samples demonstrates successful acquisition of high-quality Cl K-edge XANES spectra in fluorescence mode, high signal-to-noise Co K-edge EXAFS data in transmission mode with extended k-space coverage up to 16 Å−1, and high-sensitivity Ti K-edge fluorescence XAFS on dilute (1–3%) TiO2 polymorphs. These results confirm the system’s capability for reliable, high-precision spectroscopy across the tender-energy range (2–16 keV), supporting both trace-element analysis and detailed local-structure determination. The fully integrated system is now operational at the beamline, providing a robust platform for advanced X-ray absorption studies in environmental, catalytic, and materials science.

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Publication Details

Journal
Applied Sciences
Published
2026-05-11
DOI
https://doi.org/10.3390/app16104751
Primary Topic
X-ray Spectroscopy and Fluorescence Analysis
Type
article
Field-Weighted Citation Impact
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article

Data Acquisition System for the Tender-Energy Spectroscopy Beamline at the Shanghai Synchrotron Radiation Facility

C Hu, Y ZHAO, Zhaohong Zhang, W. J. Zhu et al.
Applied Sciences
X-ray Spectroscopy and Fluorescence Analysis
article

Data Acquisition System for the Tender-Energy Spectroscopy Beamline at the Shanghai Synchrotron Radiation Facility

C Hu, Y ZHAO, Zhaohong Zhang, W. J. Zhu, Yi Zhou, Xuying Lan, Yingfeng Wu, Chunpeng Wang, Bing Nan, Shui Liu, Huiting Chen, Lingling Guo, Jian He, Shumin Yang
article en

Abstract

A dedicated data acquisition system has been developed and commissioned for the tender-energy spectroscopy beamline BL16U1 at the Shanghai Synchrotron Radiation Facility. The system implements a distributed architecture integrating EPICS-based hardware control with the Bluesky experiment orchestration environment, supporting multiple X-ray absorption spectroscopy modes including transmission, total electron yield, total fluorescence yield, and partial fluorescence yield detection. A key technical feature is the hardware-level synchronization between a multi-channel silicon drift detector and a multichannel scaler, enabling precise timing for fluorescence-XAS measurements. A unified graphical interface based on Control System Studio provides streamlined experiment control and real-time data visualization. System validation using standard reference samples demonstrates successful acquisition of high-quality Cl K-edge XANES spectra in fluorescence mode, high signal-to-noise Co K-edge EXAFS data in transmission mode with extended k-space coverage up to 16 Å−1, and high-sensitivity Ti K-edge fluorescence XAFS on dilute (1–3%) TiO2 polymorphs. These results confirm the system’s capability for reliable, high-precision spectroscopy across the tender-energy range (2–16 keV), supporting both trace-element analysis and detailed local-structure determination. The fully integrated system is now operational at the beamline, providing a robust platform for advanced X-ray absorption studies in environmental, catalytic, and materials science.

Applied SciencesVol. 16(10)
Chinese Academy of Sciences (CN), Shanghai Advanced Research Institute (CN)
Openalex Percentile: Top 4%
X-ray Spectroscopy and Fluorescence Analysis
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