Hydrophobic Menthol‐Based Deep Eutectic Solvent for Ultrasound‐Assisted Dispersive Liquid‒Liquid Microextraction of Amide Herbicides in Food and Environmental Samples Before Determination by HPLC

) and high precision (intraday RSDs ≤ 3.6%, inter-day RSDs ≤ 8.2%). The method achieved high recoveries (89.8%-116%) across various samples. Greenness assessments using the GAREEprep and Analytical Ecological Scale showed scores of 0.57 and 85, respectively, underscoring the sustainability of the method. This study presents a rapid, sensitive, and sustainable alternative for monitoring amide herbicide residues, contributing to food safety and environmental protection.

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Publication Details

Journal
Journal of Separation Science
Published
2026-05-01
DOI
https://doi.org/10.1002/jssc.70433
Primary Topic
Analytical chemistry methods development
Type
article
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article

Hydrophobic Menthol‐Based Deep Eutectic Solvent for Ultrasound‐Assisted Dispersive Liquid‒Liquid Microextraction of Amide Herbicides in Food and Environmental Samples Before Determination by HPLC

H WANG, Guihua Ruan, Menghong Xie, Jiazhen Wei et al.
Journal of Separation Science
Analytical chemistry methods development
article

Hydrophobic Menthol‐Based Deep Eutectic Solvent for Ultrasound‐Assisted Dispersive Liquid‒Liquid Microextraction of Amide Herbicides in Food and Environmental Samples Before Determination by HPLC

H WANG, Guihua Ruan, Menghong Xie, Jiazhen Wei, Guxi Huang, Junliang Lin, Yipeng Huang
article en

Abstract

) and high precision (intraday RSDs ≤ 3.6%, inter-day RSDs ≤ 8.2%). The method achieved high recoveries (89.8%-116%) across various samples. Greenness assessments using the GAREEprep and Analytical Ecological Scale showed scores of 0.57 and 85, respectively, underscoring the sustainability of the method. This study presents a rapid, sensitive, and sustainable alternative for monitoring amide herbicide residues, contributing to food safety and environmental protection.

Journal of Separation ScienceVol. 49(5)
Guilin University of Technology (CN)
Openalex Percentile: Top 8%
Analytical chemistry methods development
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