Effect of Solution Treatment Temperature on Microstructural Evolution and Mechanical Properties of GH4698 Superalloy

This study systematically investigates the effects of solution temperature ranging from 1060 to 1150 °C on grain growth kinetics, microstructural evolution, and tensile properties of GH4698 superalloys. The results indicate that grain size coarsens parabolically with increasing solution temperature. Based on the Sellars model, the grain growth time exponent n is determined to be 3.4 and the activation energy Q is 478.7 kJ·mol−1. This confirms that the grain growth process is significantly influenced by both MC carbide pinning and alloying element drag effects. Additionally, due to the coarsening of grains, the precipitation density of M23C6 carbides per unit grain boundary length increased from 0.26 μm−1 to 0.39 μm−1. The ultimate tensile strength at room temperature decreased from 1268 MPa to 1226 MPa, and the yield strength decreased from 840 MPa to 807 MPa, while the elongation remained at 28–32%. At 700 °C, the ultimate tensile strength decreases from 974 MPa to 904 MPa, and the yield strength decreases from 755 MPa to 696 MPa, with the elongation remaining at ~6%. Quantitative analysis reveals that the decrease in strength is primarily due to the weakening of grain boundary strengthening caused by grain coarsening. At 700 °C, the deformation mechanism transitions from dislocation shearing at room temperature to stacking fault shearing. This not only leads to a reduction in strength but also, accompanied by grain boundary weakening, results in a decrease in elongation.

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Publication Details

Journal
Materials
Published
2026-04-29
DOI
https://doi.org/10.3390/ma19091806
Primary Topic
High Temperature Alloys and Creep
Type
article
Field-Weighted Citation Impact
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article

Effect of Solution Treatment Temperature on Microstructural Evolution and Mechanical Properties of GH4698 Superalloy

Xiaofeng Yan, Jianxin Dong, He Jiang
Materials
High Temperature Alloys and Creep
article

Effect of Solution Treatment Temperature on Microstructural Evolution and Mechanical Properties of GH4698 Superalloy

Xiaofeng Yan, Jianxin Dong, He Jiang
article en

Abstract

This study systematically investigates the effects of solution temperature ranging from 1060 to 1150 °C on grain growth kinetics, microstructural evolution, and tensile properties of GH4698 superalloys. The results indicate that grain size coarsens parabolically with increasing solution temperature. Based on the Sellars model, the grain growth time exponent n is determined to be 3.4 and the activation energy Q is 478.7 kJ·mol−1. This confirms that the grain growth process is significantly influenced by both MC carbide pinning and alloying element drag effects. Additionally, due to the coarsening of grains, the precipitation density of M23C6 carbides per unit grain boundary length increased from 0.26 μm−1 to 0.39 μm−1. The ultimate tensile strength at room temperature decreased from 1268 MPa to 1226 MPa, and the yield strength decreased from 840 MPa to 807 MPa, while the elongation remained at 28–32%. At 700 °C, the ultimate tensile strength decreases from 974 MPa to 904 MPa, and the yield strength decreases from 755 MPa to 696 MPa, with the elongation remaining at ~6%. Quantitative analysis reveals that the decrease in strength is primarily due to the weakening of grain boundary strengthening caused by grain coarsening. At 700 °C, the deformation mechanism transitions from dislocation shearing at room temperature to stacking fault shearing. This not only leads to a reduction in strength but also, accompanied by grain boundary weakening, results in a decrease in elongation.

MaterialsVol. 19(9)
China Iron and Steel Research Institute Group (CN), University of Science and Technology Beijing (CN)
State Administration for Science, Technology and Industry for National Defense
Openalex Percentile: Top 10%
High Temperature Alloys and Creep
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