Assessment of between-bottle homogeneity, particle size, and element content of candidate reference materials of black cricket (Gryllus assimilis) employing energy-dispersive X-ray fluorescence spectrometry
). Coefficients of variation were below 11%, and expanded uncertainties remained under 30%. These results demonstrate adequate precision, reproducibility, and matrix suitability of the proposed material. The study supports continued evaluation of intra-bottle homogeneity, stability, and certification to enable its availability for laboratories performing elemental analysis of cricket-based foods, strengthening analytical reliability and food safety assessment in emerging insect protein chains worldwide. This contribution addresses national needs and supports sustainable nutrition research efforts.
Authors
- Elvis Joacir de França (ORCID: https://orcid.org/0000-0002-0027-2028)
- MARIA JOSÉ DE FILGUEIRAS GOMES
- R Soares Pereira
- Vinícius Humberto da Silva Bezerra
Institutions
- Centro de Tecnologias Estratégicas do Nordeste (BR)
- Universidade Federal Rural de Pernambuco (BR)
Publication Details
- Journal
- Analytical and Bioanalytical Chemistry
- Published
- 2026-05-02
- DOI
- https://doi.org/10.1007/s00216-026-06503-4
- Primary Topic
- Insect Utilization and Effects
- Type
- article
- Field-Weighted Citation Impact
- 0.00