Assessment of between-bottle homogeneity, particle size, and element content of candidate reference materials of black cricket (Gryllus assimilis) employing energy-dispersive X-ray fluorescence spectrometry

). Coefficients of variation were below 11%, and expanded uncertainties remained under 30%. These results demonstrate adequate precision, reproducibility, and matrix suitability of the proposed material. The study supports continued evaluation of intra-bottle homogeneity, stability, and certification to enable its availability for laboratories performing elemental analysis of cricket-based foods, strengthening analytical reliability and food safety assessment in emerging insect protein chains worldwide. This contribution addresses national needs and supports sustainable nutrition research efforts.

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Publication Details

Journal
Analytical and Bioanalytical Chemistry
Published
2026-05-02
DOI
https://doi.org/10.1007/s00216-026-06503-4
Primary Topic
Insect Utilization and Effects
Type
article
Field-Weighted Citation Impact
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article

Assessment of between-bottle homogeneity, particle size, and element content of candidate reference materials of black cricket (Gryllus assimilis) employing energy-dispersive X-ray fluorescence spectrometry

Elvis Joacir de França, MARIA JOSÉ DE FILGUEIRAS GOMES, R Soares Pereira, Vinícius Humberto da Silva Bezerra
Analytical and Bioanalytical Chemistry
Insect Utilization and Effects
article

Assessment of between-bottle homogeneity, particle size, and element content of candidate reference materials of black cricket (Gryllus assimilis) employing energy-dispersive X-ray fluorescence spectrometry

Elvis Joacir de França, MARIA JOSÉ DE FILGUEIRAS GOMES, R Soares Pereira, Vinícius Humberto da Silva Bezerra
article en

Abstract

). Coefficients of variation were below 11%, and expanded uncertainties remained under 30%. These results demonstrate adequate precision, reproducibility, and matrix suitability of the proposed material. The study supports continued evaluation of intra-bottle homogeneity, stability, and certification to enable its availability for laboratories performing elemental analysis of cricket-based foods, strengthening analytical reliability and food safety assessment in emerging insect protein chains worldwide. This contribution addresses national needs and supports sustainable nutrition research efforts.

Analytical and Bioanalytical Chemistry
Centro de Tecnologias Estratégicas do Nordeste (BR), Universidade Federal Rural de Pernambuco (BR)
Zero hunger
Openalex Percentile: Top 11%
Insect Utilization and Effects
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Assessment of between-bottle homogeneity, particle size, and element content of candidate reference materials of black cricket (Gryllus assimilis) employing energy-dispersive X-ray fluorescence spectrometry — Elvis Joacir de França, MARIA JOSÉ DE FILGUEIRAS GOMES, et al. · Analytical and Bioanalytical Chemistry (2026) | TGRS Research Map | TGRS