Dual-precipitates enhance fatigue resistance in an additively manufactured high-entropy alloy

To accomplish the intense desire of high-strength materials for enhanced energy-efficiency, recent research applies a combined strategy of additive-manufacturing and precipitation-strengthening in high entropy alloys. In a context, Al0.2Co1.5CrFeNi1.5Ti0.3 nanoprecipitation-strengthened system was developed, demonstrating very convincing strength and toughness. Moreover, additive-manufacturing facilitated additional strength by well-decorated cell-boundaries with blocky L21 precipitates and homogeneously distributed L12 precipitates. However, fatigue research of this alloy remained unexplored despite being the main precursor for structural applications. In this study low-cycle fatigue behavior of this alloy in both as-built and precipitation-strengthened (aged) conditions has been explored, combined with in-situ neutron diffraction investigation. Findings revealed a substantial cyclic-stress profile and a notable fatigue-life below ±0.50% strain-amplitude, exceeding 105 cycles at ±0.30% strain-amplitude. These demonstrate the potential to carry higher payloads with marked engineering-reliability. Residual-stress estimation revealed strain-compatibility between the matrix and L12 precipitate, indicating a crack-initiation immune interface. A comparative examination of dislocation character revealed shifting towards pure edge-character in aged alloy indicates precipitates promoted planar-slip during deformation. The demand for high-strength materials to enhance energy efficiency drives research into additive manufacturing and precipitation strengthening of high entropy alloys. Here, the authors investigate the low-cycle fatigue behavior of an Al-Co-Cr-Fe-Ni-Ti alloy, revealing impressive fatigue life and stress profiles, highlighting its potential for reliable structural applications.

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Publication Details

Journal
Communications Materials
Published
2026-04-28
DOI
https://doi.org/10.1038/s43246-026-01129-6
Primary Topic
High Entropy Alloys Studies
Type
article
Field-Weighted Citation Impact
0.00

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article

Dual-precipitates enhance fatigue resistance in an additively manufactured high-entropy alloy

S E Lee, Mao-Yuan Luo, Lia Amalia, An‐Chou Yeh et al.
Communications Materials
High Entropy Alloys Studies
article

Dual-precipitates enhance fatigue resistance in an additively manufactured high-entropy alloy

S E Lee, Mao-Yuan Luo, Lia Amalia, An‐Chou Yeh, Jai Jain, Po-Heng Chou, E‐Wen Huang, Sudhanshu Shekhar Singh, Shuo-Ting Hsu, Tu‐Ngoc Lam, Ke An, Dunji Yu, Peter K. Liaw, Poresh Kumar, Jing-Syuan Lai, Winson C. H. Kuo, Yan Chen
article en

Abstract

To accomplish the intense desire of high-strength materials for enhanced energy-efficiency, recent research applies a combined strategy of additive-manufacturing and precipitation-strengthening in high entropy alloys. In a context, Al0.2Co1.5CrFeNi1.5Ti0.3 nanoprecipitation-strengthened system was developed, demonstrating very convincing strength and toughness. Moreover, additive-manufacturing facilitated additional strength by well-decorated cell-boundaries with blocky L21 precipitates and homogeneously distributed L12 precipitates. However, fatigue research of this alloy remained unexplored despite being the main precursor for structural applications. In this study low-cycle fatigue behavior of this alloy in both as-built and precipitation-strengthened (aged) conditions has been explored, combined with in-situ neutron diffraction investigation. Findings revealed a substantial cyclic-stress profile and a notable fatigue-life below ±0.50% strain-amplitude, exceeding 105 cycles at ±0.30% strain-amplitude. These demonstrate the potential to carry higher payloads with marked engineering-reliability. Residual-stress estimation revealed strain-compatibility between the matrix and L12 precipitate, indicating a crack-initiation immune interface. A comparative examination of dislocation character revealed shifting towards pure edge-character in aged alloy indicates precipitates promoted planar-slip during deformation. The demand for high-strength materials to enhance energy efficiency drives research into additive manufacturing and precipitation strengthening of high entropy alloys. Here, the authors investigate the low-cycle fatigue behavior of an Al-Co-Cr-Fe-Ni-Ti alloy, revealing impressive fatigue life and stress profiles, highlighting its potential for reliable structural applications.

Communications Materials
Oak Ridge National Laboratory (US), Los Alamos National Laboratory (US), National Yang Ming Chiao Tung University (TW), Chungnam National University (KR), National Tsing Hua University (TW), Vinh Long University of Technology Education (VN), Center for Integrated Nanotechnologies (US), Indian Institute of Technology Delhi (IN), University of Tennessee at Knoxville (US), Indian Institute of Technology Kanpur (IN)
National Science Foundation, U.S. Department of Energy, Center for Integrated Nanotechnologies, National Research Foundation, Indian Institute of Technology Kanpur, Shanghai Educational Development Foundation, Ministry of Education, India, National Tsing Hua University, National Synchrotron Radiation Research Center, National Science and Technology Council, Office of Science, National Nuclear Security Administration, Division of Materials Research, Army Research Office, Oak Ridge National Laboratory, Los Alamos National Laboratory
Affordable and clean energy
Openalex Percentile: Top 12%
High Entropy Alloys Studies
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