Finely Pulverized Low‐Moisture (FPL) Gel‐State NMR for Near‐Completely Solubilized Whole Plant Cell Walls
(4:1, v/v) solvent system produces gels with reproducible chemical shifts, narrow linewidths, and well-resolved heteronuclear correlations. This stability allows standard automated shimming and acquisition protocols to be applied reliably. The method is validated across diverse types of biomass, establishing a robust NMR sample-preparation framework for whole plant cell wall analysis and extending the practical reach of solution-state NMR methodologies.
Authors
- Daniel J. Yelle (ORCID: https://orcid.org/0000-0001-5321-6778)
- Peter Kitin (ORCID: https://orcid.org/0000-0002-4717-7108)
- Hoon Kim (ORCID: https://orcid.org/0000-0001-7425-7464)
- José C. del Rı́o (ORCID: https://orcid.org/0000-0002-3040-6787)
- Jorge Rencoret (ORCID: https://orcid.org/0000-0003-2728-7331)
- Yimin Mao
Institutions
- Florida A&M University - Florida State University College of Engineering (US)
- Forest Products Laboratory (US)
- Instituto de Recursos Naturales y Agrobiología de Sevilla (ES)
Publication Details
- Journal
- Magnetic Resonance in Chemistry
- Published
- 2026-04-16
- DOI
- https://doi.org/10.1002/mrc.70106
- Primary Topic
- Polysaccharides and Plant Cell Walls
- Type
- article
- Field-Weighted Citation Impact
- 0.00
Funders
- European Regional Development Fund