Comparison of Microstructure and Mechanical Properties of Ti65 Alloy Prepared by Micro and Conventional Laser Powder Bed Fusion

The demand for miniaturized high-temperature components necessitates advanced additive manufacturing techniques, yet the microstructural and mechanical consequences of scaling down the laser powder bed fusion (LPBF) process remain poorly understood. In this study, we systematically investigate the scaling effects of micro laser powder bed fusion (μ-LPBF) versus conventional LPBF on the phase transformation kinetics and performance of the near-α Ti65 alloy. Results demonstrate that μ-LPBF significantly enhances surface integrity, reducing the arithmetic mean roughness (Ra) by 59.5%. Microstructural characterization reveals that the extreme cooling rates intrinsic to the microscale melt pool induce a massive refinement of hierarchical α′ martensite and promote a highly randomized variant selection. Consequently, the strong building-direction crystallographic texture typical of LPBF is substantially weakened, and the proportion of high-angle grain boundaries increases to 91.6%. This microstructural homogenization effectively mitigates mechanical anisotropy, reducing the directional variance in the Schmid factor by 35%. In terms of mechanical properties, μ-LPBF demonstrates exceptional strengthening at both room temperature and 600 °C, achieving a room-temperature yield strength of 1297 MPa and an ultimate tensile strength of 1514 MPa, which represent increases of 16.5% and 8.6%, respectively, compared to those of conventional LPBF. These findings provide critical insights into defect suppression and multiscale microstructural control under extreme thermal gradients, paving the way for the fabrication of isotropic, high-strength micro devices.