Dry Sliding Adhesion and Wear Behavior of LPBF Ti-6Al-4V ELI (Grade 23): Influence of In-Layer Remelting on Microstructure, Surface Integrity, and Tribolayer Stability

Laser Powder Bed Fusion (LPBF) enables the fabrication of complex titanium alloy components with high geometric freedom; however, surface integrity and tribological performance remain critical limitations for sliding-contact applications in biomedical and aerospace systems. In this study, the influence of in-layer laser remelting on the microstructure, surface topography, and dry sliding tribological behavior of LPBF-fabricated Ti-6Al-4V ELI (Grade 23) is systematically investigated. Disc-shaped specimens were produced using single-scan (SS) and double-scan (DS, in-layer remelting) strategies and tested in ball-on-disc configuration against AISI 52100 steel at a constant normal load of 10 N and three sliding speeds of 0.10, 0.15, and 0.20 m·s−1. Microstructural and phase-related characteristics were analyzed by X-ray diffraction combined with Rietveld refinement and Warren–Averbach analysis, revealing that the DS strategy increases retained β-phase fraction (up to 5.2%) and promotes crystallite coarsening relative to the SS condition, without significantly altering bulk hardness. Surface morphology examined by SEM/EDS and AFM revealed a more homogeneous near-surface topography in the DS condition. Tribological results indicate that sliding speed governs steady-state friction and wear, with specific wear rates increasing progressively from 5.13 to 5.44 × 10−4 mm3·N−1·m−1 for SS and from 6.47 to 7.52 × 10−4 mm3·N−1·m−1 for DS across the investigated speed range. The DS specimens exhibited higher wear rates than the SS condition across all tested speeds, while steady-state COF values remained comparable between strategies, indicating that remelting-induced microstructural modifications affect material removal mechanisms without proportionally destabilizing the frictional regime. These findings suggest that in-layer laser remelting represents a process-integrated parameter with measurable consequences for surface integrity and tribological performance, though the generalizability of these results warrants validation across broader experimental conditions.