Nitrogen Content Effects on Microstructural Evolution and Low-Temperature Impact Toughness in the Coarse-Grained Heat-Affected Zone of Welded X70 Pipeline Steel

The low-temperature toughness of a coarse-grained heat-affected zone (CGHAZ) is a critical factor governing the service safety of welded joints in X70 pipeline steel. This study systematically investigated the influence of nitrogen content (ranging from 0.0018 to 0.0120 wt%) on the microstructure and low-temperature impact toughness of the CGHAZ in X70 pipeline steel using welding thermal simulation tests with a heat input of 12.5 kJ/cm. The results indicate that the CGHAZ microstructure predominantly comprises lath bainite (LB) and minor martensite–austenite (M/A) constituents. With increasing nitrogen content, the austenite-to-ferrite transformation start temperature (Ar3) increased while the transformation finish temperature (Ar1) decreased, resulting in coarsening of the lath bainite packet structure. The M/A volume fraction rose from 2.11% to 5.23%, the average particle size grew from 0.17 to 0.71 μm, and the high-angle grain boundary (HAGB > 15°) fraction declined from 67.5% to 52.2%. These microstructural alterations collectively caused the Charpy impact energy of the CGHAZ to decrease from 269 J to 48 J. The deterioration in toughness is primarily attributed to blocky M-A constituents lowering the resistance to crack nucleation and the reduced HAGB fraction diminishing the resistance to crack propagation. This work provides a theoretical foundation for optimizing the performance of X70 pipeline steel welded joints, and it is recommended that the nitrogen content in the base metal be strictly maintained below 0.005 wt% to ensure superior CGHAZ toughness.

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Publication Details

Journal
Metals
Published
2026-03-16
DOI
https://doi.org/10.3390/met16030331
Primary Topic
Microstructure and Mechanical Properties of Steels
Type
article
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article

Nitrogen Content Effects on Microstructural Evolution and Low-Temperature Impact Toughness in the Coarse-Grained Heat-Affected Zone of Welded X70 Pipeline Steel

Tiansheng Wang, Hu Ma, Jiangli He, Qingfeng Wang et al.
Metals
Microstructure and Mechanical Properties of Steels
article

Nitrogen Content Effects on Microstructural Evolution and Low-Temperature Impact Toughness in the Coarse-Grained Heat-Affected Zone of Welded X70 Pipeline Steel

Tiansheng Wang, Hu Ma, Jiangli He, Qingfeng Wang, Jiangcheng Liu, Chuanyou Zhang, Kai Guo, Junchao Wang
article en

Abstract

The low-temperature toughness of a coarse-grained heat-affected zone (CGHAZ) is a critical factor governing the service safety of welded joints in X70 pipeline steel. This study systematically investigated the influence of nitrogen content (ranging from 0.0018 to 0.0120 wt%) on the microstructure and low-temperature impact toughness of the CGHAZ in X70 pipeline steel using welding thermal simulation tests with a heat input of 12.5 kJ/cm. The results indicate that the CGHAZ microstructure predominantly comprises lath bainite (LB) and minor martensite–austenite (M/A) constituents. With increasing nitrogen content, the austenite-to-ferrite transformation start temperature (Ar3) increased while the transformation finish temperature (Ar1) decreased, resulting in coarsening of the lath bainite packet structure. The M/A volume fraction rose from 2.11% to 5.23%, the average particle size grew from 0.17 to 0.71 μm, and the high-angle grain boundary (HAGB > 15°) fraction declined from 67.5% to 52.2%. These microstructural alterations collectively caused the Charpy impact energy of the CGHAZ to decrease from 269 J to 48 J. The deterioration in toughness is primarily attributed to blocky M-A constituents lowering the resistance to crack nucleation and the reduced HAGB fraction diminishing the resistance to crack propagation. This work provides a theoretical foundation for optimizing the performance of X70 pipeline steel welded joints, and it is recommended that the nitrogen content in the base metal be strictly maintained below 0.005 wt% to ensure superior CGHAZ toughness.

MetalsVol. 16(3)
Yanshan University (CN), Henan Polytechnic University (CN)
Openalex Percentile: Top 21%
Microstructure and Mechanical Properties of Steels
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