Defects, Microstructure, and Hardness of As-Built and Heat-Treated 13 Hot Work Tool Steel and 17-4 PH Stainless Steel Obtained by Fused Filament Fabrication

Fused Filament Fabrication (FFF) is a low-cost additive manufacturing process that produces metallic parts from printing with a metal-polymer filament, followed by a debinding–sintering process. It presents an opportunity for the tooling sector to improve performance by geometrical optimization while keeping costs low. This study investigates the possibility of producing a molding core for plastic injection by FFF technology. This research aimed to characterize 17-4 PH stainless steel and H13 hot work tool steels produced through this process. Their heat treatment behavior was investigated using dilatometry, which led to the obtention of a Continuous Cooling Transformation (CCT) diagram. Results show that for as-sintered materials, martensitic steel with some residual austenite is present in 17-4 PH, and a pearlitic microstructure is observed in H13. Porosity (around 4%) falls within the reported range in the literature and can be removed by hot isostatic pressing. CCT diagrams do not show significant differences with conventional materials. The low hardness of as-sintered H13 (around 175 HV1) is improved (>500 HV1) by suitable heat treatment. Finally, both materials meet the requirements for this specific industrial application, and demonstrators were produced.

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Publication Details

Journal
Journal of Manufacturing and Materials Processing
Published
2026-02-27
DOI
https://doi.org/10.3390/jmmp10030084
Primary Topic
Injection Molding Process and Properties
Type
article
Field-Weighted Citation Impact
0.00

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article

Defects, Microstructure, and Hardness of As-Built and Heat-Treated 13 Hot Work Tool Steel and 17-4 PH Stainless Steel Obtained by Fused Filament Fabrication

Morgane Mokhtari, Yannick Balcaen, Joël Alexis, David López-Bolaños et al.
Journal of Manufacturing and Materials Processing
Injection Molding Process and Properties
article

Defects, Microstructure, and Hardness of As-Built and Heat-Treated 13 Hot Work Tool Steel and 17-4 PH Stainless Steel Obtained by Fused Filament Fabrication

Morgane Mokhtari, Yannick Balcaen, Joël Alexis, David López-Bolaños, Chirag Khandivar
article en

Abstract

Fused Filament Fabrication (FFF) is a low-cost additive manufacturing process that produces metallic parts from printing with a metal-polymer filament, followed by a debinding–sintering process. It presents an opportunity for the tooling sector to improve performance by geometrical optimization while keeping costs low. This study investigates the possibility of producing a molding core for plastic injection by FFF technology. This research aimed to characterize 17-4 PH stainless steel and H13 hot work tool steels produced through this process. Their heat treatment behavior was investigated using dilatometry, which led to the obtention of a Continuous Cooling Transformation (CCT) diagram. Results show that for as-sintered materials, martensitic steel with some residual austenite is present in 17-4 PH, and a pearlitic microstructure is observed in H13. Porosity (around 4%) falls within the reported range in the literature and can be removed by hot isostatic pressing. CCT diagrams do not show significant differences with conventional materials. The low hardness of as-sintered H13 (around 175 HV1) is improved (>500 HV1) by suitable heat treatment. Finally, both materials meet the requirements for this specific industrial application, and demonstrators were produced.

Journal of Manufacturing and Materials ProcessingVol. 10(3)
Centro de Estudios e Investigaciones Técnicas de Gipuzkoa (ES), Laboratoire Génie de Production (FR), Universidad de Navarra (ES)
European Synchrotron Radiation Facility, Interreg
Openalex Percentile: Top 42%
Injection Molding Process and Properties
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