Effect of Pressure and Temperature on the Microstructure and Vickers Microhardness of the CoCrFeMnNiAl1.5 Alloy During Conventional Sintering and High-Frequency Induction Sintering

This study evaluates the effects of sintering time and applied pressure on the microstructure and Vickers microhardness of the CoCrFeMnNiAl1.5 alloy during consolidation. Samples were obtained by mechanical alloying and consolidated using two routes: conventional sintering (CS) and high-frequency induction sintering followed by high-temperature heating (HFIHS + HTH). For both methods, the pressure (0.3–1.5 GPa) and holding time (1–4 h) were varied. The results show that the HFIHS + HTS route produces a finer microstructure, with notably more homogeneous Cr segregation at high pressures, resulting in higher Vickers hardness values (up to 770 HV). In addition, the pressure applied during HFIHS promotes a mechanism of forced atomic mobility. This mechanism facilitates the migration of atoms toward energetically favorable sites, such as grain boundaries. At the same time, it restricts precipitate growth and Cr-rich segregation and activates densification mechanisms without requiring sustained pressure. The optimal parameters (0.9 GPa and 1 h) produce the best microstructural and mechanical response, highlighting the potential of this alloy for use in coatings and structural components in the automotive and aerospace industries.

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Publication Details

Journal
Coatings
Published
2026-02-26
DOI
https://doi.org/10.3390/coatings16030275
Primary Topic
Advanced materials and composites
Type
article
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article

Effect of Pressure and Temperature on the Microstructure and Vickers Microhardness of the CoCrFeMnNiAl1.5 Alloy During Conventional Sintering and High-Frequency Induction Sintering

José Luis Hernández Rivera, Audel Santos Beltrán, Gustavo Rodriguez Cabriales, José Manuel Mendoza Duarte et al.
Coatings
Advanced materials and composites
article

Effect of Pressure and Temperature on the Microstructure and Vickers Microhardness of the CoCrFeMnNiAl1.5 Alloy During Conventional Sintering and High-Frequency Induction Sintering

José Luis Hernández Rivera, Audel Santos Beltrán, Gustavo Rodriguez Cabriales, José Manuel Mendoza Duarte, A. García, Roberto Martínez Sánchez, Hansel Manuel Medrano Prieto, Carlos Gamaliel Garay Reyes, Ivanovich Estrada Guel, Enrique Rocha Rangel, Leonardo Baylón García
article en

Abstract

This study evaluates the effects of sintering time and applied pressure on the microstructure and Vickers microhardness of the CoCrFeMnNiAl1.5 alloy during consolidation. Samples were obtained by mechanical alloying and consolidated using two routes: conventional sintering (CS) and high-frequency induction sintering followed by high-temperature heating (HFIHS + HTH). For both methods, the pressure (0.3–1.5 GPa) and holding time (1–4 h) were varied. The results show that the HFIHS + HTS route produces a finer microstructure, with notably more homogeneous Cr segregation at high pressures, resulting in higher Vickers hardness values (up to 770 HV). In addition, the pressure applied during HFIHS promotes a mechanism of forced atomic mobility. This mechanism facilitates the migration of atoms toward energetically favorable sites, such as grain boundaries. At the same time, it restricts precipitate growth and Cr-rich segregation and activates densification mechanisms without requiring sustained pressure. The optimal parameters (0.9 GPa and 1 h) produce the best microstructural and mechanical response, highlighting the potential of this alloy for use in coatings and structural components in the automotive and aerospace industries.

CoatingsVol. 16(3)
Autonomous University of Chihuahua (MX), Autonomous University of San Luis Potosí (MX), Tecnológico Nacional de México (MX), Secretaría de Ciencia Tecnología e Innovación (MX), Centro de Investigación en Materiales Avanzados (MX), Universidad Tecnológica de Chihuahua
Openalex Percentile: Top 43%
Advanced materials and composites
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