Development and characterization of cinnamon essential oil – incorporated kudzu starch – based biodegradable films for food packaging applications

Kudzu starch, owing to its excellent film-forming capability, is a promising biodegradable alternative to conventional plastic packaging. In this study, kudzu starch films were fabricated using glycerol and beeswax to enhance flexibility and hydrophobicity, achieving a maximum water contact angle of 116°and a reduced water vapor permeability (WVP) of 1 . 75 ± 0 . 34 × 1 0 − 10 g m m −2 s −1 Pa −1 . The optimized film exhibited a Young’s modulus of 4 . 00 ± 0 . 59 MPa , indicating improved mechanical integrity suitable for food-packaging applications. Antibacterial functionality was introduced by incorporating cinnamon essential oil at concentrations of 1%–3%. The films exhibited significant antibacterial activity against Escherichia coli ( E. coli ), with an inhibition zone diameter reaching 20 . 3 ± 2 . 1 mm at 3% essential oil content. Microstructural and physicochemical analyses using FE-SEM, water absorption, moisture retention, and biodegradation tests confirmed effective modification of the starch matrix. Practical food-packaging performance was evaluated using strawberries as model samples, where films containing 3% cinnamon essential oil significantly reduced the total aerobic bacterial count to 5.75 log 10 CFU/g after 6 days of storage, compared with 7.51 log 10 CFU/g for nylon packaging, and extended the shelf life to 9 days versus 5 days for conventional nylon packaging. These results demonstrate that kudzu starch-based films provide enhanced barrier, antibacterial, and preservation performance, highlighting their strong potential as sustainable food-packaging materials. • Kudzu starch was employed to fabricate biodegradable films for food-packaging applications. • Glycerol and beeswax significantly enhanced the flexibility and hydrophobicity of the films. • Beeswax surface modification increased the water contact angle to as high as 116°. • Kudzu starch films incorporated with cinnamon essential oil exhibited strong antibacterial activity against E. coli . • Strawberries coated with the developed films showed prolonged shelf life and reduced microbial spoilage.

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Publication Details

Journal
Next Materials
Published
2026-02-25
DOI
https://doi.org/10.1016/j.nxmate.2026.101790
Primary Topic
Nanocomposite Films for Food Packaging
Type
article
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article

Development and characterization of cinnamon essential oil – incorporated kudzu starch – based biodegradable films for food packaging applications

Thi Quyen Ha, Bao Long Hoang, Thi Thao Vu, Thi Ngoc Minh Dinh et al.
Next Materials
Nanocomposite Films for Food Packaging
article

Development and characterization of cinnamon essential oil – incorporated kudzu starch – based biodegradable films for food packaging applications

Thi Quyen Ha, Bao Long Hoang, Thi Thao Vu, Thi Ngoc Minh Dinh, Thi Hoa Hoang, Duc Cuong Nguyen
article en

Abstract

Kudzu starch, owing to its excellent film-forming capability, is a promising biodegradable alternative to conventional plastic packaging. In this study, kudzu starch films were fabricated using glycerol and beeswax to enhance flexibility and hydrophobicity, achieving a maximum water contact angle of 116°and a reduced water vapor permeability (WVP) of 1 . 75 ± 0 . 34 × 1 0 − 10 g m m −2 s −1 Pa −1 . The optimized film exhibited a Young’s modulus of 4 . 00 ± 0 . 59 MPa , indicating improved mechanical integrity suitable for food-packaging applications. Antibacterial functionality was introduced by incorporating cinnamon essential oil at concentrations of 1%–3%. The films exhibited significant antibacterial activity against Escherichia coli ( E. coli ), with an inhibition zone diameter reaching 20 . 3 ± 2 . 1 mm at 3% essential oil content. Microstructural and physicochemical analyses using FE-SEM, water absorption, moisture retention, and biodegradation tests confirmed effective modification of the starch matrix. Practical food-packaging performance was evaluated using strawberries as model samples, where films containing 3% cinnamon essential oil significantly reduced the total aerobic bacterial count to 5.75 log 10 CFU/g after 6 days of storage, compared with 7.51 log 10 CFU/g for nylon packaging, and extended the shelf life to 9 days versus 5 days for conventional nylon packaging. These results demonstrate that kudzu starch-based films provide enhanced barrier, antibacterial, and preservation performance, highlighting their strong potential as sustainable food-packaging materials. • Kudzu starch was employed to fabricate biodegradable films for food-packaging applications. • Glycerol and beeswax significantly enhanced the flexibility and hydrophobicity of the films. • Beeswax surface modification increased the water contact angle to as high as 116°. • Kudzu starch films incorporated with cinnamon essential oil exhibited strong antibacterial activity against E. coli . • Strawberries coated with the developed films showed prolonged shelf life and reduced microbial spoilage.

Next MaterialsVol. 11
Vietnam National University, Hanoi (VN), VNU University of Science (VN)
Zero hunger
Openalex Percentile: Top 45%
Nanocomposite Films for Food Packaging
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