Novel Quantification of Non-convex Grain Morphology in Printed Ti–6Al–4V

Abstract Complete and accurate quantification of additively manufactured microstructures, along with all their relevant features, is essential for reliable model development, calibration and qualification. This study analyzed trends in grain size and shape in a set of orientation maps acquired from samples of LPBF Ti–6Al–4V printed with varying power and scan speed, all within the process window. The EBSD maps of the $$\alpha $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>α</mml:mi> </mml:math> phase were used to reconstruct the parent $$\beta $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>β</mml:mi> </mml:math> grain structure. Fitting a convex hull around each $$\beta $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>β</mml:mi> </mml:math> grain and computing solidity was found to be effective in capturing the non-traditional morphology of the AM microstructures and their asymmetry with respect to the build direction. An equivalent synthetically generated microstructure with similar grain size and aspect ratio was used for comparison of the developed metrics between it and the AM-fabricated samples. The comparison shows that the aspect ratio fails to capture the morphological complexity of AM microstructures, whereas the new metrics effectively differentiate the two types of microstructures. Other than a slight variation in grain size, the grain shape exhibits negligible variation across the range of processing conditions explored.

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Publication Details

Journal
Metallurgical and Materials Transactions A
Published
2026-02-24
DOI
https://doi.org/10.1007/s11661-026-08159-2
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
Field-Weighted Citation Impact
0.00

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article

Novel Quantification of Non-convex Grain Morphology in Printed Ti–6Al–4V

G. Wong, Leo A. I. Kestens, Tuan Nguyen-Minh, Ioannis Dalezios
Metallurgical and Materials Transactions A
Additive Manufacturing Materials and Processes
article

Novel Quantification of Non-convex Grain Morphology in Printed Ti–6Al–4V

G. Wong, Leo A. I. Kestens, Tuan Nguyen-Minh, Ioannis Dalezios
article en

Abstract

Abstract Complete and accurate quantification of additively manufactured microstructures, along with all their relevant features, is essential for reliable model development, calibration and qualification. This study analyzed trends in grain size and shape in a set of orientation maps acquired from samples of LPBF Ti–6Al–4V printed with varying power and scan speed, all within the process window. The EBSD maps of the $$\alpha $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>α</mml:mi> </mml:math> phase were used to reconstruct the parent $$\beta $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>β</mml:mi> </mml:math> grain structure. Fitting a convex hull around each $$\beta $$ <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"> <mml:mi>β</mml:mi> </mml:math> grain and computing solidity was found to be effective in capturing the non-traditional morphology of the AM microstructures and their asymmetry with respect to the build direction. An equivalent synthetically generated microstructure with similar grain size and aspect ratio was used for comparison of the developed metrics between it and the AM-fabricated samples. The comparison shows that the aspect ratio fails to capture the morphological complexity of AM microstructures, whereas the new metrics effectively differentiate the two types of microstructures. Other than a slight variation in grain size, the grain shape exhibits negligible variation across the range of processing conditions explored.

Metallurgical and Materials Transactions A
HOGENT University of Applied Sciences and Arts (BE), Ghent University (BE), Carnegie Mellon University (US)
National Aeronautics and Space Administration, Carnegie Mellon University, Nuclear Safety and Security Commission, Alexander S. Onassis Public Benefit Foundation, Smithsonian Tropical Research Institute
Openalex Percentile: Top 46%
Additive Manufacturing Materials and Processes
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