Thermally Induced Creep and Viscoelastic Behavior of Copper Micropillar Arrays

Copper micropillar arrays integrated in microchannel structures promise superior heat dissipation, yet their long-term reliability can be limited by creep deformation under thermomechanical constraints. Here, we fabricate Cu micropillar arrays (∼50 µm in diameter and ∼300 µm in height) via electrodeposition within through-glass vias (TGVs) and elucidate how heat treatment tailors creep, viscoelastic response, and deformation mechanisms. Nanoindentation creep combined with EBSD and TEM reveals the transition: 200°C promotes grain-boundary-mediated deformation with the largest creep displacement (101 nm) and the smallest activation volume (0.64 nm<sup>3</sup>), whereas 300°C increases dislocation density and produces dislocation pile-ups/networks that pin grain boundaries, reducing creep displacement to 42 nm, raising the stress exponent to 3.76, and the activation volume recovers to 1.49 nm<sup>3</sup>. Viscoelasticity is quantified with a generalized Kelvin model and retardation spectrum analysis, which shows suppressed relaxation activity after 300°C treatment. Thermal tests on arrays with varying pitch indicate that 70 µm spacing yields the most pronounced monitored-surface temperature rise (46.5°C) under identical heating, implying enhanced effective heat transport through the micropillar network. These results establish a microstructure-mechanism-property framework to guide the design of Cu micropillar arrays that balance manufacturability, creep reliability, and thermal performance for microscale liquid-cooling.

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Publication Details

Journal
Advanced Science
Published
2026-02-17
DOI
https://doi.org/10.1002/advs.202519178
Primary Topic
Microstructure and mechanical properties
Type
article
Field-Weighted Citation Impact
0.00

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article

Thermally Induced Creep and Viscoelastic Behavior of Copper Micropillar Arrays

Wenbo Luo, M. X. Wang, Mingcheng Chen, Xingzhou Cai et al.
Advanced Science
Microstructure and mechanical properties
article

Thermally Induced Creep and Viscoelastic Behavior of Copper Micropillar Arrays

Wenbo Luo, M. X. Wang, Mingcheng Chen, Xingzhou Cai, Dongbin Wang, Wanli Zhang, Ting Liu, Shuang Li, Hongwei Chen, Libin Gao, Mengru Li, Jihua Zhang, Bin Peng, Yong Li, Wenlei Li
article en

Abstract

Copper micropillar arrays integrated in microchannel structures promise superior heat dissipation, yet their long-term reliability can be limited by creep deformation under thermomechanical constraints. Here, we fabricate Cu micropillar arrays (∼50 µm in diameter and ∼300 µm in height) via electrodeposition within through-glass vias (TGVs) and elucidate how heat treatment tailors creep, viscoelastic response, and deformation mechanisms. Nanoindentation creep combined with EBSD and TEM reveals the transition: 200°C promotes grain-boundary-mediated deformation with the largest creep displacement (101 nm) and the smallest activation volume (0.64 nm<sup>3</sup>), whereas 300°C increases dislocation density and produces dislocation pile-ups/networks that pin grain boundaries, reducing creep displacement to 42 nm, raising the stress exponent to 3.76, and the activation volume recovers to 1.49 nm<sup>3</sup>. Viscoelasticity is quantified with a generalized Kelvin model and retardation spectrum analysis, which shows suppressed relaxation activity after 300°C treatment. Thermal tests on arrays with varying pitch indicate that 70 µm spacing yields the most pronounced monitored-surface temperature rise (46.5°C) under identical heating, implying enhanced effective heat transport through the micropillar network. These results establish a microstructure-mechanism-property framework to guide the design of Cu micropillar arrays that balance manufacturability, creep reliability, and thermal performance for microscale liquid-cooling.

Advanced Science
University of Electronic Science and Technology of China (CN), Dongguan University of Technology (CN), National Engineering Research Center of Electromagnetic Radiation Control Materials (CN), Chengdu Tiger Microwave Technology (China) (CN)
National Key Research and Development Program of China
Openalex Percentile: Top 53%
Microstructure and mechanical properties
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