The Effect of Cementation Load, Unload Time, and Storage Time on Film Thickness and Microtensile Bond Strength Durability of Dual-Cure Resin Cements: An In Vitro Study
This article aims to evaluate the effect of load weight, unload time, and storage duration on microtensile bond strength (µTBS) of dual-cure resin cement to CAD/CAM composite.Forty-eight composite blocks (Grandio Blocs, <i>n</i> = 24 shade A1, and <i>n</i> = 24 shade A4) were randomly assigned to eight groups (<i>n</i> = 3 shade A1, and <i>n</i> = 3 shade A4) based on load weight (1, 3, 5, and 15 kg), and unload time (immediately before light curing or 10 minutes during/after light curing). Bonded blocks (<i>n</i> = 3/group) were sectioned into multiple sticks. Half of the sticks (<i>n</i> = 21) were tested after 24 hours, while the remaining 21 were stored in distilled water at 37°C and tested after 6 months. Sticks for film thickness were evaluated using a stereomicroscope (60 × ). However, the sticks for µTBS were pulled in tension at a 0.5-mm/min crosshead speed.Data were analyzed using ANOVA and the Games-Howell post hoc test (<i>α</i> = 0.05).There was no correlation between µTBS and FT (<i>r</i> = 0.035; <i>p</i> = 0.737). For the FT, only "unload time" had a significant effect (<i>p</i> < 0.001). For µTBS, "load weight," and "unload time" had no significant impact (<i>p</i> = 0.948 and <i>p</i> = 0.948, respectively). However, "storage time" significantly influenced the results (<i>p</i> < 0.001). Adhesive mode was significantly predominant (56.85%).Unload time is a crucial factor controlling the film thickness of the dual-cure resin cement. However, it does not affect the resin cement µTBS to CAD/CAM composite.Excessive seating load should be avoided when positioning CAD/CAM composite restorations, while a controlled short time may assist in preventing restoration rebound.
Authors
- Salvatore Sauro (ORCID: https://orcid.org/0000-0002-2527-8776)
- Sara Adel Botros (ORCID: https://orcid.org/0000-0001-8169-2528)
- Nader Tadros
- Abdullah Hassanien
- Farid S. El-Askary
Institutions
- Ain Shams University (EG)
- British University in Egypt (EG)
- Sechenov University (RU)
- Universidad Cardenal Herrera CEU (ES)
- Egyptian Russian University (EG)
Publication Details
- Journal
- European Journal of Dentistry
- Published
- 2026-02-16
- DOI
- https://doi.org/10.1055/s-0046-1816082
- Primary Topic
- Dental materials and restorations
- Type
- article
- Field-Weighted Citation Impact
- 0.00