Effect of Adatom Energy on the Interfacial and Surface Morphology of Pulsed DC Sputtered Ruthenium Thin Films

ABSTRACT In the present study, we have analyzed the growth profile of ruthenium (Ru) thin films, deposited using pulsed direct current (DC) magnetron sputtering technique, by varying the sputtering voltages in the range of 150–420 V. The grazing incidence X‐ray reflectivity (GIXRR), time‐of‐flight secondary ion mass spectrometry (ToF‐SIMS), and atomic force microscopy (AFM) techniques were employed to determine the interface characteristics and surface morphology. A pronounced Ru diffusion was found inside the substrate region with an increase in sputtering voltage, and the density and roughness of the interfacial layer also increased. The surface roughness was found to increase from 0.28 to 2.6 nm. Details of the growth profile as determined from the GIXRR and SIMS measurements are discussed.

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Publication Details

Journal
Surface and Interface Analysis
Published
2026-02-12
DOI
https://doi.org/10.1002/sia.70060
Primary Topic
Ion-surface interactions and analysis
Type
article
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article

Effect of Adatom Energy on the Interfacial and Surface Morphology of Pulsed DC Sputtered Ruthenium Thin Films

Mohammed H. Modi, Rajiv Kamparath, Shruti Gupta, A. Chandra Bose et al.
Surface and Interface Analysis
Ion-surface interactions and analysis
article

Effect of Adatom Energy on the Interfacial and Surface Morphology of Pulsed DC Sputtered Ruthenium Thin Films

Mohammed H. Modi, Rajiv Kamparath, Shruti Gupta, A. Chandra Bose, R. K. Gupta, P. K. Yadav, C. Mukherjee
article en

Abstract

ABSTRACT In the present study, we have analyzed the growth profile of ruthenium (Ru) thin films, deposited using pulsed direct current (DC) magnetron sputtering technique, by varying the sputtering voltages in the range of 150–420 V. The grazing incidence X‐ray reflectivity (GIXRR), time‐of‐flight secondary ion mass spectrometry (ToF‐SIMS), and atomic force microscopy (AFM) techniques were employed to determine the interface characteristics and surface morphology. A pronounced Ru diffusion was found inside the substrate region with an increase in sputtering voltage, and the density and roughness of the interfacial layer also increased. The surface roughness was found to increase from 0.28 to 2.6 nm. Details of the growth profile as determined from the GIXRR and SIMS measurements are discussed.

Surface and Interface Analysis
Raja Ramanna Centre for Advanced Technology (IN), Homi Bhabha National Institute (IN)
Affordable and clean energy
Openalex Percentile: Top 54%
Ion-surface interactions and analysis
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Effect of Adatom Energy on the Interfacial and Surface Morphology of Pulsed DC Sputtered Ruthenium Thin Films — Mohammed H. Modi, Rajiv Kamparath, et al. · Surface and Interface Analysis (2026) | TGRS Research Map | TGRS