Texture Evolution and In Situ Investigation of Recrystallization Behavior in a Hot-Rolled Al-Zn-Mg-Cu-Zr Alloy

By means of characterization techniques such as XRD, TEM, and in situ EBSD, the texture evolution, recrystallization behavior, and their modulation by the Al<sub>3</sub>Zr phase in hot-rolled Al-Zn-Mg-Cu-Zr alloys with varied homogenization treatments were investigated. Results show that both the single-stage homogenized (SH) alloy and the double-stage homogenized (DH) alloy acquired a typical β-fiber texture after hot rolling, including brass, S, and copper orientations. The DH alloy experienced suppressed recrystallization (a recrystallization fraction of 6.05%) owing to its higher density of Al<sub>3</sub>Zr precipitates. In contrast, the SH alloy exhibited more significant dissolution and agglomeration of Al<sub>3</sub>Zr, leading to extensive recrystallization peaking at 78.1%. The primary recrystallization mode was identified as continuous recrystallization, characterized by the growth and coarsening of subgrains. Although dynamically recrystallized (DRx) grains formed during hot rolling could act as potential recrystallization nuclei, most of them exhibited weak growth capability, except the cube-oriented grains. During recrystallization, deformed grains with S orientation tended to transform into cube-oriented grains, while those with brass orientation prefer to convert into Goss-oriented grains. This can be attributed to the presence of highly mobile grain boundaries between these specific orientation pairs. In the DH alloy, subgrain growth and DRx grain consumption during annealing reduced orientation dispersion in deformed grains, promoting marked brass texture strengthening, with its volume fraction reaching 57.7%.

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Journal
Materials
Published
2026-02-09
DOI
https://doi.org/10.3390/ma19040665
Primary Topic
Aluminum Alloy Microstructure Properties
Type
article
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article

Texture Evolution and In Situ Investigation of Recrystallization Behavior in a Hot-Rolled Al-Zn-Mg-Cu-Zr Alloy

Jianfei Hao, Yuchong Hu, Huang Huilan, Runxia Li et al.
Materials
Aluminum Alloy Microstructure Properties
article

Texture Evolution and In Situ Investigation of Recrystallization Behavior in a Hot-Rolled Al-Zn-Mg-Cu-Zr Alloy

Jianfei Hao, Yuchong Hu, Huang Huilan, Runxia Li, Peng Xia, Kedu Lin
article en

Abstract

By means of characterization techniques such as XRD, TEM, and in situ EBSD, the texture evolution, recrystallization behavior, and their modulation by the Al<sub>3</sub>Zr phase in hot-rolled Al-Zn-Mg-Cu-Zr alloys with varied homogenization treatments were investigated. Results show that both the single-stage homogenized (SH) alloy and the double-stage homogenized (DH) alloy acquired a typical β-fiber texture after hot rolling, including brass, S, and copper orientations. The DH alloy experienced suppressed recrystallization (a recrystallization fraction of 6.05%) owing to its higher density of Al<sub>3</sub>Zr precipitates. In contrast, the SH alloy exhibited more significant dissolution and agglomeration of Al<sub>3</sub>Zr, leading to extensive recrystallization peaking at 78.1%. The primary recrystallization mode was identified as continuous recrystallization, characterized by the growth and coarsening of subgrains. Although dynamically recrystallized (DRx) grains formed during hot rolling could act as potential recrystallization nuclei, most of them exhibited weak growth capability, except the cube-oriented grains. During recrystallization, deformed grains with S orientation tended to transform into cube-oriented grains, while those with brass orientation prefer to convert into Goss-oriented grains. This can be attributed to the presence of highly mobile grain boundaries between these specific orientation pairs. In the DH alloy, subgrain growth and DRx grain consumption during annealing reduced orientation dispersion in deformed grains, promoting marked brass texture strengthening, with its volume fraction reaching 57.7%.

MaterialsVol. 19(4)
Dongguan University of Technology (CN), Guangdong Academy of Sciences (CN), Institute of New Materials (CN), Chongqing Three Gorges University (CN)
Openalex Percentile: Top 62%
Aluminum Alloy Microstructure Properties
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Texture Evolution and In Situ Investigation of Recrystallization Behavior in a Hot-Rolled Al-Zn-Mg-Cu-Zr Alloy — Jianfei Hao, Yuchong Hu, et al. · Materials (2026) | TGRS Research Map | TGRS