In-situ tensile SEM investigation on the high-temperature tensile properties and deformation mechanism in Ti-6Al-4V alloy with different microstructure types

To reveal the influence of microstructure types on high-temperature tensile properties and deformation mechanism in TC4 titanium alloy, this work conducted tensile tests and in-situ tensile SEM observation at 350°C on the as-received equiaxed microstructure (EM), the designed lamellar microstructure (LM) and two types (I and Ⅱ) of bimodal microstructures with similar equiaxed α (α eq ) phase content. Wherein, Type I had a colony structure consisting of lamellar α and interlayer β. Type Ⅱ had a bilamellar structure consisting of basketweave-α and dispersed α. The high-temperature tensile and in-situ tensile results showed that Types I and Ⅱ had higher strength than EM and LM, which could be attributed to that more interfaces fabricated in Types I and Ⅱ to restrict slip transfer and hinder dislocation movement. Moreover, Type Ⅱ had higher strength than Type Ⅰ due to precipitation strengthening. The EM had the highest plasticity, which could be attributed to that α eq grains could accommodate more plastic deformation through the initiation of multiple slip and twins. The LM had the lowest strength and plasticity. This is because during early deformation, coarse α-colonies in the LM tended to induce crack nucleation at α-colony/colony and α-colony/grain boundary α interfaces, which would be detrimental to strength and plasticity. Additionally, compared to room-temperature tensile deformation, high-temperature tensile deformation exhibited better work hardening ability with increasing strain due to the formation of massive dislocation networks, dislocation tangles and twins.

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Journal
Journal of Materials Research and Technology
Published
2026-02-04
DOI
https://doi.org/10.1016/j.jmrt.2026.02.029
Primary Topic
Titanium Alloys Microstructure and Properties
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article
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article

In-situ tensile SEM investigation on the high-temperature tensile properties and deformation mechanism in Ti-6Al-4V alloy with different microstructure types

Honghui Li, Ke Wang, Le Feng
Journal of Materials Research and Technology
Titanium Alloys Microstructure and Properties
article

In-situ tensile SEM investigation on the high-temperature tensile properties and deformation mechanism in Ti-6Al-4V alloy with different microstructure types

Honghui Li, Ke Wang, Le Feng
article en

Abstract

To reveal the influence of microstructure types on high-temperature tensile properties and deformation mechanism in TC4 titanium alloy, this work conducted tensile tests and in-situ tensile SEM observation at 350°C on the as-received equiaxed microstructure (EM), the designed lamellar microstructure (LM) and two types (I and Ⅱ) of bimodal microstructures with similar equiaxed α (α eq ) phase content. Wherein, Type I had a colony structure consisting of lamellar α and interlayer β. Type Ⅱ had a bilamellar structure consisting of basketweave-α and dispersed α. The high-temperature tensile and in-situ tensile results showed that Types I and Ⅱ had higher strength than EM and LM, which could be attributed to that more interfaces fabricated in Types I and Ⅱ to restrict slip transfer and hinder dislocation movement. Moreover, Type Ⅱ had higher strength than Type Ⅰ due to precipitation strengthening. The EM had the highest plasticity, which could be attributed to that α eq grains could accommodate more plastic deformation through the initiation of multiple slip and twins. The LM had the lowest strength and plasticity. This is because during early deformation, coarse α-colonies in the LM tended to induce crack nucleation at α-colony/colony and α-colony/grain boundary α interfaces, which would be detrimental to strength and plasticity. Additionally, compared to room-temperature tensile deformation, high-temperature tensile deformation exhibited better work hardening ability with increasing strain due to the formation of massive dislocation networks, dislocation tangles and twins.

Journal of Materials Research and TechnologyVol. 41
Chongqing University (CN)
Openalex Percentile: Top 68%
Titanium Alloys Microstructure and Properties
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