The Effect of Laser Surface Hardening on the Microstructural Characteristics and Wear Resistance of 9CrSi Steel

This study presents a systematic investigation of laser surface hardening of 9CrSi tool steel with the aim of establishing the relationships between processing parameters, microstructural evolution, and resulting mechanical and tribological properties under the applied laser conditions. The influence of laser power, modulation frequency, and scanning speed on the hardened layer depth, microstructure, and surface properties was analyzed. Laser treatment produced a martensitic surface layer with varying fractions of retained austenite, while the transition zone consisted of martensite, granular pearlite, and carbide particles. X-ray diffraction identified the presence of α'-Fe, γ-Fe, and Fe<sub>3</sub>C phases, with peak broadening associated with increased lattice microstrain induced by rapid self-quenching. The surface microhardness increased from approximately 220 HV<sub>0.1</sub> in the untreated state to 950-1000 HV<sub>0.1</sub> after laser hardening, with hardened layer thicknesses ranging from about 500 to 750 µm depending on the processing regime. Instrumented indentation showed higher elastic modulus values for all hardened conditions. Tribological tests under dry sliding conditions revealed reduced coefficients of friction and more than an order-of-magnitude decrease in wear rate compared with untreated steel. The results provide a parameter-microstructure-performance map for laser-hardened 9CrSi steel, demonstrating how variations in laser processing conditions affect hardened layer characteristics and functional performance.

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Publication Details

Journal
Materials
Published
2026-01-21
DOI
https://doi.org/10.3390/ma19020423
Citations
1
Primary Topic
High Entropy Alloys Studies
Type
article
Field-Weighted Citation Impact
19.05
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article

The Effect of Laser Surface Hardening on the Microstructural Characteristics and Wear Resistance of 9CrSi Steel

Zhuldyz Sagdoldina, S.D. Bolatov, Daryn Baizhan, Dastan Buitkenov et al.
1 citations
Materials
High Entropy Alloys Studies
19.05
article

The Effect of Laser Surface Hardening on the Microstructural Characteristics and Wear Resistance of 9CrSi Steel

Zhuldyz Sagdoldina, S.D. Bolatov, Daryn Baizhan, Dastan Buitkenov, Aibek Alibekov, Gulim Tleubergenova
article en
1 citations

Abstract

This study presents a systematic investigation of laser surface hardening of 9CrSi tool steel with the aim of establishing the relationships between processing parameters, microstructural evolution, and resulting mechanical and tribological properties under the applied laser conditions. The influence of laser power, modulation frequency, and scanning speed on the hardened layer depth, microstructure, and surface properties was analyzed. Laser treatment produced a martensitic surface layer with varying fractions of retained austenite, while the transition zone consisted of martensite, granular pearlite, and carbide particles. X-ray diffraction identified the presence of α'-Fe, γ-Fe, and Fe<sub>3</sub>C phases, with peak broadening associated with increased lattice microstrain induced by rapid self-quenching. The surface microhardness increased from approximately 220 HV<sub>0.1</sub> in the untreated state to 950-1000 HV<sub>0.1</sub> after laser hardening, with hardened layer thicknesses ranging from about 500 to 750 µm depending on the processing regime. Instrumented indentation showed higher elastic modulus values for all hardened conditions. Tribological tests under dry sliding conditions revealed reduced coefficients of friction and more than an order-of-magnitude decrease in wear rate compared with untreated steel. The results provide a parameter-microstructure-performance map for laser-hardened 9CrSi steel, demonstrating how variations in laser processing conditions affect hardened layer characteristics and functional performance.

MaterialsVol. 19(2)
Sarsen Amanzholov East Kazakhstan University (KZ), Shakarim University (KZ)
Openalex Percentile: Top 2%
High Entropy Alloys Studies
19.05
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The Effect of Laser Surface Hardening on the Microstructural Characteristics and Wear Resistance of 9CrSi Steel — Zhuldyz Sagdoldina, S.D. Bolatov, et al. · Materials (2026) | TGRS Research Map | TGRS