Fabricating irradiation-tolerant ODS Fe-Cr steel with engineered Y-Ti-O nanoprecipitates by laser powder bed fusion

• Highly dense ODS Fe-Cr steel components were prepared by LPBF. • Uniformly dispersed Y-Ti-O nanoprecipitates with high density were in situ constructed. • Superior radiation tolerance and mechanical properties were achieved via tailored microstructures. • High-quality interfaces between Y-Ti-O nanoprecipitates and Fe-Cr matrix improved radiation tolerance and creep resistance. Developing advanced structural materials for next-generation nuclear reactors that simultaneously achieve superior radiation tolerance, excellent mechanical properties, and manufacturable components remains a significant challenge. Additive manufacturing via laser powder bed fusion (LPBF) offers a promising pathway to engineer high-performance reactor materials with tailored microstructures. Herein, oxide dispersion-strengthened (ODS) Fe-Cr steels with near-full density (>99 %) and uniformly dispersed Y-Ti-O nanoprecipitates (number density approximately 4 × 10 20 /m 3 ) were fabricated by LPBF using gas-atomized reaction-synthesized powders. In-situ formed Y-Ti-O nanoprecipitates during the intrinsic heat treatment of the LPBF process enhanced the energy barrier to plastic deformation in ODS Fe-Cr steel by impeding dislocation motion and climb, thereby conferring superior high-temperature strength and creep resistance compared to the Fe-Cr steel counterpart. Furthermore, energetic Au + and He + ion irradiations, coupled with transmission electron microscopy and nanoindentation analyses, demonstrate that the LPBF-engineered high-density interfaces between Y-Ti-O nanoparticles and the Fe-Cr matrix serve as efficient sinks for irradiation-induced defects. This interface-mediated defect annihilation mechanism mitigated radiation damage, ensured microstructural stability, and reduced irradiation hardening. This work provides valuable insights into the design and manufacturing of irradiation-resistant ODS steel components via LPBF for advanced nuclear reactors.

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Publication Details

Journal
Materials & Design
Published
2026-01-08
DOI
https://doi.org/10.1016/j.matdes.2026.115466
Primary Topic
Fusion materials and technologies
Type
article
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article

Fabricating irradiation-tolerant ODS Fe-Cr steel with engineered Y-Ti-O nanoprecipitates by laser powder bed fusion

Shuyao Si, Yiqiang Zhong, Langlang Zhao, Jun Tang et al.
Materials & Design
Fusion materials and technologies
article

Fabricating irradiation-tolerant ODS Fe-Cr steel with engineered Y-Ti-O nanoprecipitates by laser powder bed fusion

Shuyao Si, Yiqiang Zhong, Langlang Zhao, Jun Tang, Jie Li, Guangxu Cai, Feng Ren, Nannan Jia, Lulu Hu, Wei Teng, Wenhao Yang
article en

Abstract

• Highly dense ODS Fe-Cr steel components were prepared by LPBF. • Uniformly dispersed Y-Ti-O nanoprecipitates with high density were in situ constructed. • Superior radiation tolerance and mechanical properties were achieved via tailored microstructures. • High-quality interfaces between Y-Ti-O nanoprecipitates and Fe-Cr matrix improved radiation tolerance and creep resistance. Developing advanced structural materials for next-generation nuclear reactors that simultaneously achieve superior radiation tolerance, excellent mechanical properties, and manufacturable components remains a significant challenge. Additive manufacturing via laser powder bed fusion (LPBF) offers a promising pathway to engineer high-performance reactor materials with tailored microstructures. Herein, oxide dispersion-strengthened (ODS) Fe-Cr steels with near-full density (>99 %) and uniformly dispersed Y-Ti-O nanoprecipitates (number density approximately 4 × 10 20 /m 3 ) were fabricated by LPBF using gas-atomized reaction-synthesized powders. In-situ formed Y-Ti-O nanoprecipitates during the intrinsic heat treatment of the LPBF process enhanced the energy barrier to plastic deformation in ODS Fe-Cr steel by impeding dislocation motion and climb, thereby conferring superior high-temperature strength and creep resistance compared to the Fe-Cr steel counterpart. Furthermore, energetic Au + and He + ion irradiations, coupled with transmission electron microscopy and nanoindentation analyses, demonstrate that the LPBF-engineered high-density interfaces between Y-Ti-O nanoparticles and the Fe-Cr matrix serve as efficient sinks for irradiation-induced defects. This interface-mediated defect annihilation mechanism mitigated radiation damage, ensured microstructural stability, and reduced irradiation hardening. This work provides valuable insights into the design and manufacturing of irradiation-resistant ODS steel components via LPBF for advanced nuclear reactors.

Materials & DesignVol. 262
Wuhan University (CN), Jiuquan Iron & Steel (China) (CN), Frontier Energy (United States) (US), Xi'an Jiaotong University (CN)
Affordable and clean energy
Openalex Percentile: Top 93%
Fusion materials and technologies
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