Variability in elastic and corrosion properties with laser scan speed in selective-laser-melted 316L SS

The large parameter space of selective laser melting (SLM) presents a challenge for property predictors. In this work, the complete set of elastic moduli and the corrosion behavior were determined and correlated for SLM-316L stainless steel. Standard volumetric energy density ranged from 56 to 83 J/mm 3 , with 100 W laser power, 50 m laser spot size, 60 m hatch space, 25 m powder layer thickness, and laser scanning speed varied between 800 and 1200 mm/s. Location-dependent elastic properties were determined with resonant ultrasound spectroscopy on mm-sized rectangular parallelepipeds. Pulse-echo provided a volume-integrated longitudinal modulus. Cyclic potentiodynamic polarization measurements were used to determine the corrosion potential, pitting potential, repassivation current, and corrosion current density. Electron Backscatter Diffraction fund that high-angle grain boundary density dominates at 1200 mm/s, with a high value of 0.46 / , more than four-fold larger than the low-angle grain boundary density. The 1200 mm/s (mass density =0.985 ) has lower corrosion resistance, with highest I =45 nA/cm 2 and lowest E =0.45 V, but elastically is closest to volumetrically isotropic, with compressional moduli of 223.69 8.53 GPa and shear moduli of 72.49 0.36 GPa. At 800 mm/s (mass density = ) the material has the highest crystallographic texture, but a delayed onset to pitting and the greatest resistance to corrosion. Elastically it is not isotropic and degeneracy among directions relative to the build-direction is found. The range of properties observed, understood through grain boundary density and misorientation distribution analysis, reinforces SLM’s capabilities: tuning of SLM fabrication parameters enables materials tailoring for optimal performance in specific applications. • Volumetric elastic isotropy in 316L is possible by selective laser melting at 100 W and 1200 mm/s. • Change in the scan speed of 100 W SLM-316L can tune its corrosion resistance and elastic anisotropy. • Elastic, corrosion, and microstructure properties correlate quantitatively in 100 W SLM-316L. • Resonant ultrasound can map elastic properties of additively manufactured alloys in detail.

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Journal
Materials Today Communications
Published
2026-01-07
DOI
https://doi.org/10.1016/j.mtcomm.2025.114583
Primary Topic
Additive Manufacturing Materials and Processes
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article
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article

Variability in elastic and corrosion properties with laser scan speed in selective-laser-melted 316L SS

Matthew A. Steiner, Mason Hayward, Md Shafayet Alam, Gabriela Petculescu et al.
Materials Today Communications
Additive Manufacturing Materials and Processes
article

Variability in elastic and corrosion properties with laser scan speed in selective-laser-melted 316L SS

Matthew A. Steiner, Mason Hayward, Md Shafayet Alam, Gabriela Petculescu, Erica Perry Murray, Likun Sun
article en

Abstract

The large parameter space of selective laser melting (SLM) presents a challenge for property predictors. In this work, the complete set of elastic moduli and the corrosion behavior were determined and correlated for SLM-316L stainless steel. Standard volumetric energy density ranged from 56 to 83 J/mm 3 , with 100 W laser power, 50 m laser spot size, 60 m hatch space, 25 m powder layer thickness, and laser scanning speed varied between 800 and 1200 mm/s. Location-dependent elastic properties were determined with resonant ultrasound spectroscopy on mm-sized rectangular parallelepipeds. Pulse-echo provided a volume-integrated longitudinal modulus. Cyclic potentiodynamic polarization measurements were used to determine the corrosion potential, pitting potential, repassivation current, and corrosion current density. Electron Backscatter Diffraction fund that high-angle grain boundary density dominates at 1200 mm/s, with a high value of 0.46 / , more than four-fold larger than the low-angle grain boundary density. The 1200 mm/s (mass density =0.985 ) has lower corrosion resistance, with highest I =45 nA/cm 2 and lowest E =0.45 V, but elastically is closest to volumetrically isotropic, with compressional moduli of 223.69 8.53 GPa and shear moduli of 72.49 0.36 GPa. At 800 mm/s (mass density = ) the material has the highest crystallographic texture, but a delayed onset to pitting and the greatest resistance to corrosion. Elastically it is not isotropic and degeneracy among directions relative to the build-direction is found. The range of properties observed, understood through grain boundary density and misorientation distribution analysis, reinforces SLM’s capabilities: tuning of SLM fabrication parameters enables materials tailoring for optimal performance in specific applications. • Volumetric elastic isotropy in 316L is possible by selective laser melting at 100 W and 1200 mm/s. • Change in the scan speed of 100 W SLM-316L can tune its corrosion resistance and elastic anisotropy. • Elastic, corrosion, and microstructure properties correlate quantitatively in 100 W SLM-316L. • Resonant ultrasound can map elastic properties of additively manufactured alloys in detail.

Materials Today CommunicationsVol. 51
University of Cincinnati (US), University of Louisiana at Lafayette (US), Louisiana Tech University (US)
Affordable and clean energy
Openalex Percentile: Top 94%
Additive Manufacturing Materials and Processes
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