Experimental-ML frameworks for thermo-mechanical characterization of rubberized cement mortar after elevated temperature exposure

• 150 specimens were tested in compression and flexure to examine the thermo-mechanical behavior of rubberized cement mortar • DIC and ML models are employed to understand the influence of temperature on mixing proportions • Slow-cooled specimens recovered up to 20.1% more flexural strength than that obtained for instant-shock • Post-peak residual strength is enhanced by CR inclusion • Failure pattern transitioned from brittle to ductile in CR-incorporated mortar. This study presents a comprehensive experimental and data-driven investigation involving 150 specimens to evaluate the post-high-temperature thermo-mechanical behavior of rubberized cement mortar through compressive and flexural strength testing. Five mortar mixes are prepared, including a control (0% CR) and four mixes with 5%, 10%, 15%, and 20% CR by replacing NFA. Specimens are subjected to room temperature, 100°C, and 200°C, followed by immediate testing after thermal shock or slow cooling, enabling a systematic assessment of residual performance in high-temperature behavior. The findings of this investigation reveal that the compressive strength of rubberized mortar cubes decreased significantly with increasing CR content, with the highest reduction at 20% CR. At elevated temperatures, slow-cooled specimens recovered up to 20.1% more flexural strength than instant-shock counterparts, owing to improved stress redistribution and microcrack mitigation for 20% CR content. Notably, 5% CR replacement demonstrates comparable strength to the control mix while achieving superior strain accommodation and post-peak residual strength. Therefore, Digital Image Correlation (DIC) and Scanning Electron Microscopy (SEM) analyses are conducted on 5% CR beam specimens to quantify full-field strain evolution, crack development and microstructural damage mechanisms to further reinforce the experimental findings. Moreover, the current study presents the first machine learning-based approach toward estimating the flexural strength of rubberized cement mortar together with the impact level of temperature exposure, the post-heating testing environment, and the amount of CR%, with the results confirming that CR% influence is more prominent than the temperature on the flexural strength of rubberized mortar. However, this integrated experimental–DIC–SEM–ML framework represents a significant advancement over existing studies and may serve as a foundation for the optimized use of CR in thermally-exposed structural applications.

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Journal
Results in Engineering
Published
2026-01-02
DOI
https://doi.org/10.1016/j.rineng.2026.108959
Primary Topic
Fire effects on concrete materials
Type
article
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article

Experimental-ML frameworks for thermo-mechanical characterization of rubberized cement mortar after elevated temperature exposure

Tanvir Hassan Tusher, Syed Ishtiaq Ahmad, Jannatul Ferdowsi, Khondaker Sakil Ahmed et al.
Results in Engineering
Fire effects on concrete materials
article

Experimental-ML frameworks for thermo-mechanical characterization of rubberized cement mortar after elevated temperature exposure

Tanvir Hassan Tusher, Syed Ishtiaq Ahmad, Jannatul Ferdowsi, Khondaker Sakil Ahmed, Al Shahariar Fahim
article en

Abstract

• 150 specimens were tested in compression and flexure to examine the thermo-mechanical behavior of rubberized cement mortar • DIC and ML models are employed to understand the influence of temperature on mixing proportions • Slow-cooled specimens recovered up to 20.1% more flexural strength than that obtained for instant-shock • Post-peak residual strength is enhanced by CR inclusion • Failure pattern transitioned from brittle to ductile in CR-incorporated mortar. This study presents a comprehensive experimental and data-driven investigation involving 150 specimens to evaluate the post-high-temperature thermo-mechanical behavior of rubberized cement mortar through compressive and flexural strength testing. Five mortar mixes are prepared, including a control (0% CR) and four mixes with 5%, 10%, 15%, and 20% CR by replacing NFA. Specimens are subjected to room temperature, 100°C, and 200°C, followed by immediate testing after thermal shock or slow cooling, enabling a systematic assessment of residual performance in high-temperature behavior. The findings of this investigation reveal that the compressive strength of rubberized mortar cubes decreased significantly with increasing CR content, with the highest reduction at 20% CR. At elevated temperatures, slow-cooled specimens recovered up to 20.1% more flexural strength than instant-shock counterparts, owing to improved stress redistribution and microcrack mitigation for 20% CR content. Notably, 5% CR replacement demonstrates comparable strength to the control mix while achieving superior strain accommodation and post-peak residual strength. Therefore, Digital Image Correlation (DIC) and Scanning Electron Microscopy (SEM) analyses are conducted on 5% CR beam specimens to quantify full-field strain evolution, crack development and microstructural damage mechanisms to further reinforce the experimental findings. Moreover, the current study presents the first machine learning-based approach toward estimating the flexural strength of rubberized cement mortar together with the impact level of temperature exposure, the post-heating testing environment, and the amount of CR%, with the results confirming that CR% influence is more prominent than the temperature on the flexural strength of rubberized mortar. However, this integrated experimental–DIC–SEM–ML framework represents a significant advancement over existing studies and may serve as a foundation for the optimized use of CR in thermally-exposed structural applications.

Results in EngineeringVol. 29
Bangladesh University of Engineering and Technology (BD)
Openalex Percentile: Top 99%
Fire effects on concrete materials
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