Concentration-Dependent Rheological and Sensory Effects of Walnut Leaf Extract in Cosmetic Emulsion Creams

Background/Objectives: Understanding how plant-derived extracts influence the rheological and sensory behavior of emulsions is crucial for developing stable and consumer-appealing formulations. Although walnut leaf extract (Juglans regia L.) is recognized for its bioactive properties, its structural impact on cosmetic emulsions has not been systematically characterized. This study aimed to investigate the effect of increasing walnut leaf extract concentration on the rheological profile, mechanical integrity during application, and sensory performance of oil-in-water creams. Methods: Four emulsion formulations (F1–F4) containing 0%, 1%, 3%, and 5% walnut leaf extract were prepared using Olivem 1000 and Olivem 300 as emulsifiers. Rheological measurements included amplitude sweep, flow curve, frequency sweep, and thixotropy tests to assess viscoelasticity, flow behavior, and recovery. A sensory evaluation was conducted by trained panelists to correlate rheological parameters with perceived product attributes. Results: All formulations exhibited pseudoplastic, shear-thinning behavior in well-structured cosmetic emulsions during application. The addition of walnut extract significantly modified rheological responses: at 1% concentration, an increase in storage modulus (G′) and shear-thinning ratio (η0/η∞) indicated structural reinforcement and improved spreadability, whereas higher concentrations (3–5%) led to structural softening and faster thixotropic recovery. The frequency sweep revealed a concentration-dependent shift from elastic- to viscous-dominant behavior. Sensory analysis confirmed these trends, with higher extract levels reducing stickiness and greasiness while enhancing absorption. Conclusions: Walnut leaf extract shows a concentration-dependent influence on the rheological behavior of the emulsions, strengthening the network structure at low levels while promoting softening and faster structural recovery at higher concentrations. The strong correlation between rheological and sensory parameters underscores the potential of walnut extract as a multifunctional ingredient for designing well-structured, non-greasy, and consumer-preferred cosmetic creams.

Authors

Institutions

Publication Details

Journal
Cosmetics
Published
2025-12-26
DOI
https://doi.org/10.3390/cosmetics13010006
Primary Topic
Proteins in Food Systems
Type
article
Field-Weighted Citation Impact
0.00
Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

Concentration-Dependent Rheological and Sensory Effects of Walnut Leaf Extract in Cosmetic Emulsion Creams

Olivera Kostić, Jovana Dimitrijevic, Ana Adamović, Marina T Tomovic et al.
Cosmetics
Proteins in Food Systems
article

Concentration-Dependent Rheological and Sensory Effects of Walnut Leaf Extract in Cosmetic Emulsion Creams

Olivera Kostić, Jovana Dimitrijevic, Ana Adamović, Marina T Tomovic, Jelena Živković, Miljan Adamović, Marina Kostić, Ana Barjaktarević, Danijela Pecarski, Marijana Andjic
article en

Abstract

Background/Objectives: Understanding how plant-derived extracts influence the rheological and sensory behavior of emulsions is crucial for developing stable and consumer-appealing formulations. Although walnut leaf extract (Juglans regia L.) is recognized for its bioactive properties, its structural impact on cosmetic emulsions has not been systematically characterized. This study aimed to investigate the effect of increasing walnut leaf extract concentration on the rheological profile, mechanical integrity during application, and sensory performance of oil-in-water creams. Methods: Four emulsion formulations (F1–F4) containing 0%, 1%, 3%, and 5% walnut leaf extract were prepared using Olivem 1000 and Olivem 300 as emulsifiers. Rheological measurements included amplitude sweep, flow curve, frequency sweep, and thixotropy tests to assess viscoelasticity, flow behavior, and recovery. A sensory evaluation was conducted by trained panelists to correlate rheological parameters with perceived product attributes. Results: All formulations exhibited pseudoplastic, shear-thinning behavior in well-structured cosmetic emulsions during application. The addition of walnut extract significantly modified rheological responses: at 1% concentration, an increase in storage modulus (G′) and shear-thinning ratio (η0/η∞) indicated structural reinforcement and improved spreadability, whereas higher concentrations (3–5%) led to structural softening and faster thixotropic recovery. The frequency sweep revealed a concentration-dependent shift from elastic- to viscous-dominant behavior. Sensory analysis confirmed these trends, with higher extract levels reducing stickiness and greasiness while enhancing absorption. Conclusions: Walnut leaf extract shows a concentration-dependent influence on the rheological behavior of the emulsions, strengthening the network structure at low levels while promoting softening and faster structural recovery at higher concentrations. The strong correlation between rheological and sensory parameters underscores the potential of walnut extract as a multifunctional ingredient for designing well-structured, non-greasy, and consumer-preferred cosmetic creams.

CosmeticsVol. 13(1)
University of Kragujevac (RS), Institute for Plant Protection and Environment (RS)
Openalex Percentile: Top 34%
Proteins in Food Systems
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.