In-situ measurement of lengthening kinetics of Widmanstätten ferrite in low carbon steel

This study presents an automated image analysis framework to quantify the lengthening kinetics of Widmanstätten ferrite (WF) during continuous cooling of Fe–0.12C–2Mn steel. In-situ microstructures were captured using a high-temperature tensile testing system with confocal laser scanning microscope (HiTTS-CLSM). The framework integrates the open-source Segment Anything Model (SAM) for grain segmentation with the DeepLSD line segment detector for WF plate identification, enabling systematic analysis of 94 plates across 155 image frames. Four types of nucleation sites were observed at the specimen surface for WF plates. Surface observations showed nucleation appearing most frequently in austenite grain interiors (33 %), followed by nucleation at tips of existing WF plates (25.5 %), austenite grain boundaries (23.5 %), and allotriomorphic ferrite/austenite interphase boundaries (18 %). The measured lengthening rates ranged from 3 to 68 μ m/s within 730–630 ∘ C, falling between the maximum rates predicted under para-equilibrium (PE) and negligible partition local equilibrium (NPLE) conditions from modified Zener–Hillert equations. Statistical analysis revealed no significant differences in average lengthening rates across nucleation sites. The results also highlight that lengthening rate measurements are highly sensitive to the analysis method. This training-free approach significantly expands the scale of quantitative analysis compared to traditional manual methods and is applicable to transformations that produce sufficient surface relief and plate spacing above the effective resolution of the acquired images. • SAM and DeepLSD models enable automated ferrite plate tracking and measurement • Measured lengthening rates fall between PE and NPLE theoretical predictions • Statistical tests show no lengthening rate differences across four nucleation site types • Training-free approach significantly expands scale of quantitative analysis

Publication Details

Journal
Materials Today Communications
Published
2025-12-12
DOI
https://doi.org/10.1016/j.mtcomm.2025.114488
Primary Topic
Microstructure and Mechanical Properties of Steels
Type
article
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article

In-situ measurement of lengthening kinetics of Widmanstätten ferrite in low carbon steel

Materials Today Communications
Microstructure and Mechanical Properties of Steels
article

In-situ measurement of lengthening kinetics of Widmanstätten ferrite in low carbon steel

article en

Abstract

This study presents an automated image analysis framework to quantify the lengthening kinetics of Widmanstätten ferrite (WF) during continuous cooling of Fe–0.12C–2Mn steel. In-situ microstructures were captured using a high-temperature tensile testing system with confocal laser scanning microscope (HiTTS-CLSM). The framework integrates the open-source Segment Anything Model (SAM) for grain segmentation with the DeepLSD line segment detector for WF plate identification, enabling systematic analysis of 94 plates across 155 image frames. Four types of nucleation sites were observed at the specimen surface for WF plates. Surface observations showed nucleation appearing most frequently in austenite grain interiors (33 %), followed by nucleation at tips of existing WF plates (25.5 %), austenite grain boundaries (23.5 %), and allotriomorphic ferrite/austenite interphase boundaries (18 %). The measured lengthening rates ranged from 3 to 68 μ m/s within 730–630 ∘ C, falling between the maximum rates predicted under para-equilibrium (PE) and negligible partition local equilibrium (NPLE) conditions from modified Zener–Hillert equations. Statistical analysis revealed no significant differences in average lengthening rates across nucleation sites. The results also highlight that lengthening rate measurements are highly sensitive to the analysis method. This training-free approach significantly expands the scale of quantitative analysis compared to traditional manual methods and is applicable to transformations that produce sufficient surface relief and plate spacing above the effective resolution of the acquired images. • SAM and DeepLSD models enable automated ferrite plate tracking and measurement • Measured lengthening rates fall between PE and NPLE theoretical predictions • Statistical tests show no lengthening rate differences across four nucleation site types • Training-free approach significantly expands scale of quantitative analysis

Materials Today CommunicationsVol. 50
Openalex Percentile: Top 47%
Microstructure and Mechanical Properties of Steels
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In-situ measurement of lengthening kinetics of Widmanstätten ferrite in low carbon steel · Materials Today Communications (2025) | TGRS Research Map | TGRS