Triggering ultrastrong age‐hardening response of laser‐powder bed‐fused WE43 alloy via solid solution temperature design

Abstract Heat treatment is crucial for the optimization of additively manufactured components. Laser‐powder bed‐fused (L‐PBFed) magnesium‐rare earth (Mg‐RE) alloys are highly suitable for lightweight engineering applications because of their high specific strengths and top‐down fabrication. However, L‐PBFed Mg‐RE alloys have unique non‐equilibrium features that cause difficulty in the context of conventional heat treatments based on equilibrium phase diagrams or quasi‐equilibrium solidification; these challenges severely limit their performance. This study systematically reveals the unique governing mechanism of the solution‐treatment temperature over the precipitation evolution and age‐hardening responses of L‐PBFed WE43 alloy. The results indicate grain coarsening and increased heterogeneity following solution treatment. Under a low solution heat‐treatment temperature (400 °C), the in‐situ phases partially dissolve but coarse Mg 41 Nd 2 Y phases form; under a high solution heat‐treatment temperature (500 °C), the precipitates dissolve but the nucleation site density decreases through excessive defect annihilation. Under optimized solution treatment (450 °C), a defect network is retained via lattice distortions, which enables nucleation of shearable β′/β 1 phases and stacking faults (SFs) during aging. These shearable β′/β 1 phases and SFs impede the dislocations, as an anti‐phase boundary energy barrier is established, causing dislocation accumulation and strong strain gradients at the interfaces. Consequently, optimized solution treatment coupled with aging heat treatment yields stronger precipitation strengthening and heterodeformation‐induced strengthening owing to the higher density of shearable microstructures and growing grain‐size heterogeneity. This work elucidates solute‐defect coupling in L‐PBFed WE43 solution aging and provides new insights for the heat treatment of L‐PBFed Mg‐RE alloys.

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Publication Details

Journal
Rare Metals
Published
2025-11-20
DOI
https://doi.org/10.1007/s12598-025-03627-x
Primary Topic
Magnesium Alloys: Properties and Applications
Type
article
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article

Triggering ultrastrong age‐hardening response of laser‐powder bed‐fused WE43 alloy via solid solution temperature design

Rare Metals
Magnesium Alloys: Properties and Applications
article

Triggering ultrastrong age‐hardening response of laser‐powder bed‐fused WE43 alloy via solid solution temperature design

article en

Abstract

Abstract Heat treatment is crucial for the optimization of additively manufactured components. Laser‐powder bed‐fused (L‐PBFed) magnesium‐rare earth (Mg‐RE) alloys are highly suitable for lightweight engineering applications because of their high specific strengths and top‐down fabrication. However, L‐PBFed Mg‐RE alloys have unique non‐equilibrium features that cause difficulty in the context of conventional heat treatments based on equilibrium phase diagrams or quasi‐equilibrium solidification; these challenges severely limit their performance. This study systematically reveals the unique governing mechanism of the solution‐treatment temperature over the precipitation evolution and age‐hardening responses of L‐PBFed WE43 alloy. The results indicate grain coarsening and increased heterogeneity following solution treatment. Under a low solution heat‐treatment temperature (400 °C), the in‐situ phases partially dissolve but coarse Mg 41 Nd 2 Y phases form; under a high solution heat‐treatment temperature (500 °C), the precipitates dissolve but the nucleation site density decreases through excessive defect annihilation. Under optimized solution treatment (450 °C), a defect network is retained via lattice distortions, which enables nucleation of shearable β′/β 1 phases and stacking faults (SFs) during aging. These shearable β′/β 1 phases and SFs impede the dislocations, as an anti‐phase boundary energy barrier is established, causing dislocation accumulation and strong strain gradients at the interfaces. Consequently, optimized solution treatment coupled with aging heat treatment yields stronger precipitation strengthening and heterodeformation‐induced strengthening owing to the higher density of shearable microstructures and growing grain‐size heterogeneity. This work elucidates solute‐defect coupling in L‐PBFed WE43 solution aging and provides new insights for the heat treatment of L‐PBFed Mg‐RE alloys.

Rare MetalsVol. 44(12)
Chongqing University (CN), The University of Texas at El Paso (US), State Key Laboratory of Vehicle NVH and Safety Technology (CN), Tsinghua University (CN)
Openalex Percentile: Top 46%
Magnesium Alloys: Properties and Applications
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