Mechanochemical synthesis of β-cyclodextrin urea derivatives under reactive CO<sub>2</sub> atmosphere by Staudinger aza-Wittig reaction

Various ureido β-cyclodextrins can be easily synthesised by mechanochemistry from azido-β-cyclodextrins, carbon dioxide and amino derivatives. The reaction was carried out with short reaction times, without solvents and without thermal activation, greatly reducing the environmental impact of the synthesis.

Publication Details

Journal
LillOA (Université de Lille (University Of Lille))
Published
2025-09-04
Primary Topic
Drug Solubulity and Delivery Systems
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article
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article

Mechanochemical synthesis of β-cyclodextrin urea derivatives under reactive CO2 atmosphere by Staudinger aza-Wittig reaction

LillOA (Université de Lille (University Of Lille))
Drug Solubulity and Delivery Systems
article

Mechanochemical synthesis of β-cyclodextrin urea derivatives under reactive CO2 atmosphere by Staudinger aza-Wittig reaction

article en

Abstract

Various ureido β-cyclodextrins can be easily synthesised by mechanochemistry from azido-β-cyclodextrins, carbon dioxide and amino derivatives. The reaction was carried out with short reaction times, without solvents and without thermal activation, greatly reducing the environmental impact of the synthesis.

LillOA (Université de Lille (University Of Lille))
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Mechanochemical synthesis of β-cyclodextrin urea derivatives under reactive CO<sub>2</sub> atmosphere by Staudinger aza-Wittig reaction · LillOA (Université de Lille (University Of Lille)) (2025) | TGRS Research Map | TGRS