Large-area atomic layer deposition of titanium nitride for RF windows

High-power particle accelerators, like the Spallation Neutron Source, require reliable radio-frequency waveguide windows to transmit power while maintaining a vacuum. These windows face performance challenges due to multipacting, an electron cascade disrupting vacuum integrity. Thin TiN coatings can suppress this by reducing secondary electron emission, but traditional methods struggle to uniformly coat complex ceramic surfaces. We developed an atomic layer deposition (ALD) process to create conformal TiN films (<10 nm) at low temperatures (130°C), achieving smooth, conductive coatings with a secondary electron yield below 2.0. Collaborating with Microwave Techniques LLC and Oak Ridge National Laboratory, we designed RF windows with replaceable TiN-coated ceramic disks to improve performance and reduce downtime. In our next phase, we will scale up manufacturing and develop a modular ALD tool for in-situ coating of waveguide and SRF cavity metallic surfaces, crucial for next-generation accelerators operating at higher power. These innovations enhance efficiency, reliability, and design flexibility, advancing accelerator technology and fostering high-tech sector growth.

Publication Details

Journal
JACOW
Published
2025-11-05
DOI
https://doi.org/10.18429/jacow-ipac2025-thpb094
Primary Topic
Particle Accelerators and Free-Electron Lasers
Type
article
Field-Weighted Citation Impact
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article

Large-area atomic layer deposition of titanium nitride for RF windows

JACOW
Particle Accelerators and Free-Electron Lasers
article

Large-area atomic layer deposition of titanium nitride for RF windows

article en

Abstract

High-power particle accelerators, like the Spallation Neutron Source, require reliable radio-frequency waveguide windows to transmit power while maintaining a vacuum. These windows face performance challenges due to multipacting, an electron cascade disrupting vacuum integrity. Thin TiN coatings can suppress this by reducing secondary electron emission, but traditional methods struggle to uniformly coat complex ceramic surfaces. We developed an atomic layer deposition (ALD) process to create conformal TiN films (<10 nm) at low temperatures (130°C), achieving smooth, conductive coatings with a secondary electron yield below 2.0. Collaborating with Microwave Techniques LLC and Oak Ridge National Laboratory, we designed RF windows with replaceable TiN-coated ceramic disks to improve performance and reduce downtime. In our next phase, we will scale up manufacturing and develop a modular ALD tool for in-situ coating of waveguide and SRF cavity metallic surfaces, crucial for next-generation accelerators operating at higher power. These innovations enhance efficiency, reliability, and design flexibility, advancing accelerator technology and fostering high-tech sector growth.

JACOW
Industry, innovation and infrastructure
Openalex Percentile: Top 48%
Particle Accelerators and Free-Electron Lasers
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Large-area atomic layer deposition of titanium nitride for RF windows · JACOW (2025) | TGRS Research Map | TGRS