Flowability, shape and structure characterization of recycled particles originating from electro discharge machining of H11 alloy

• Recycled eroded particles are suitable for additive manufacturing and powder metallurgy. • Size, shape and morphology are similar to the reference, while flowability can be improved or worsened at certain stresses. • Surface roughness is small, and coarse recycled particles have the smoothest surface. • 3D shape and pore analyses of recycled particles show higher sphericities and smaller–sized pores in low proportion. There is a need in metal powder manufacturing to provide alternative supplies because the only production method is the energy– and cost–intensive melt atomization. The aim of this study is focused on recycling of metallic particles originating from electro discharge machining. Extracted particles from accumulating erosion sludges fulfill theoretically specifications of powders regarding particle size and shape. Two fractions were analyzed via laser diffraction, image analysis and electron microscopy and compared to the benchmark H 11–alloy. Bulk properties were measured and powders were investigated in a powder shear cell regarding flowability. These properties were combined with measurements of particle surface roughness in an atomic force microscope. Powders were examined by micro–computed tomography to obtain particle–discrete data. Recycled particles fulfill requirements regarding size, shape and defects. Their bulk properties align with the reference, showing improved or worsened flowability at certain stresses. Attached graphite in recycled fractions is acting simultaneously as nano–roughness and flow additive. H 11 shows an expected flow behavior, and the coarse fraction the smoothest surface. Results of sphericity values cannot support findings for roughness and flowability. Pores within particles are least present for H 11, hence recycled fractions have better pore performance compared to literature.

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Publication Details

Journal
Advanced Powder Technology
Published
2025-09-22
DOI
https://doi.org/10.1016/j.apt.2025.105064
Citations
1
Primary Topic
Erosion and Abrasive Machining
Type
article
Field-Weighted Citation Impact
1.84
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article

Flowability, shape and structure characterization of recycled particles originating from electro discharge machining of H11 alloy

1 citations
Advanced Powder Technology
Erosion and Abrasive Machining
1.84
article

Flowability, shape and structure characterization of recycled particles originating from electro discharge machining of H11 alloy

article en
1 citations

Abstract

• Recycled eroded particles are suitable for additive manufacturing and powder metallurgy. • Size, shape and morphology are similar to the reference, while flowability can be improved or worsened at certain stresses. • Surface roughness is small, and coarse recycled particles have the smoothest surface. • 3D shape and pore analyses of recycled particles show higher sphericities and smaller–sized pores in low proportion. There is a need in metal powder manufacturing to provide alternative supplies because the only production method is the energy– and cost–intensive melt atomization. The aim of this study is focused on recycling of metallic particles originating from electro discharge machining. Extracted particles from accumulating erosion sludges fulfill theoretically specifications of powders regarding particle size and shape. Two fractions were analyzed via laser diffraction, image analysis and electron microscopy and compared to the benchmark H 11–alloy. Bulk properties were measured and powders were investigated in a powder shear cell regarding flowability. These properties were combined with measurements of particle surface roughness in an atomic force microscope. Powders were examined by micro–computed tomography to obtain particle–discrete data. Recycled particles fulfill requirements regarding size, shape and defects. Their bulk properties align with the reference, showing improved or worsened flowability at certain stresses. Attached graphite in recycled fractions is acting simultaneously as nano–roughness and flow additive. H 11 shows an expected flow behavior, and the coarse fraction the smoothest surface. Results of sphericity values cannot support findings for roughness and flowability. Pores within particles are least present for H 11, hence recycled fractions have better pore performance compared to literature.

Advanced Powder TechnologyVol. 36(11)
TU Bergakademie Freiberg (DE)
Openalex Percentile: Top 10%
Erosion and Abrasive Machining
1.84
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