Effect of strain amplitude on the low cycle fatigue behavior and deformation mechanisms in alloy SU-263 at elevated temperature

The past studies in the low cycle fatigue (LCF) behavior of a γ′ strengthened nickel-based superalloy SU-263 were restricted to a maximum temperature of 923 K, though their service conditions far exceed this limit. In the present work, the LCF behavior of SU-263 is investigated at 1023 K with strain amplitude varying from ± 0.3% to ± 0.8% at 1023 K. During fatigue, the alloy displayed initial cyclic hardening followed by softening. The fatigue life decreased drastically with increasing strain amplitude. The alloy depicted gradual initial hardening at low strain amplitudes and sharp initial hardening at higher strain amplitudes, along with extensive softening until fracture. Significant increases in slip band density, stacking faults, dislocation network formation, and dislocation-dislocation and dislocation-precipitate interactions were identified as the deformation mechanisms responsible for cyclic hardening. In contrast, dislocation annihilation and shearing of γ′ precipitates were found to control cyclic softening. Dislocation-precipitate interactions were associated with looping at low strain amplitudes, while precipitate shearing occurred at high strain amplitudes. The alloy exhibited a tendency bilinear strain-life behavior in the Coffin-Manson plot with the corresponding shift in the fracture mode at ± 0.5% strain amplitude. At strain amplitudes below ± 0.5%, the alloy showed a mixed mode of failure, predominantly transgranular in nature, while at high strain amplitudes, the failure becomes predominantly intergranular.