Optimization of Delonix Regia Seed Oil Extraction using Taguchi Orthogonal Array Design

This study applied a Taguchi L9(3⁴) orthogonal array to optimize the solvent‐extraction of oil from Delonix regia (Flamboyant) seeds. Four factors seed Powder weight (40–50 g), particle size (0.6–3.35 mm), n-hexane volume (200–250 mL), and extraction time (40–50 min) were each tested at three levels. A Soxhlet apparatus at 60 °C served for all nine experimental runs. Oil yield ranged from 2.07 to 6.34 wt. %, with the highest yield of 6.35 ± 0.01 wt. % achieved at 50 g powder, particle size of 0.6 mm, N-hexane volume of 225 mL solvent at extraction time of 40 min. Signal‐to‐noise and Analysis of Variance (ANOVA) test revealed that particle size (p < 0.01) and Powder weight (p < 0.01) were the most influential parameters (ranked first and second), while solvent volume and time were less significant (p > 0.15). Findings using a linear regression model gave a yield variance of R² = 0.97. Confirmatory runs under optimized conditions reproduced the predicted yield within 0.2 % error. This approach comparatively delivers efficient oil recovery with minimal experimentation. Hence results from this study provides a robust basis for scaling up Delonix regia seed oil extraction in biodiesel and biosurfactant production.

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Publication Details

Journal
Zenodo (CERN European Organization for Nuclear Research)
Published
2025-08-04
DOI
https://doi.org/10.5281/zenodo.16742465
Primary Topic
Biodiesel Production and Applications
Type
article
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article

Optimization of Delonix Regia Seed Oil Extraction using Taguchi Orthogonal Array Design

Zenodo (CERN European Organization for Nuclear Research)
Biodiesel Production and Applications
article

Optimization of Delonix Regia Seed Oil Extraction using Taguchi Orthogonal Array Design

article en

Abstract

This study applied a Taguchi L9(3⁴) orthogonal array to optimize the solvent‐extraction of oil from Delonix regia (Flamboyant) seeds. Four factors seed Powder weight (40–50 g), particle size (0.6–3.35 mm), n-hexane volume (200–250 mL), and extraction time (40–50 min) were each tested at three levels. A Soxhlet apparatus at 60 °C served for all nine experimental runs. Oil yield ranged from 2.07 to 6.34 wt. %, with the highest yield of 6.35 ± 0.01 wt. % achieved at 50 g powder, particle size of 0.6 mm, N-hexane volume of 225 mL solvent at extraction time of 40 min. Signal‐to‐noise and Analysis of Variance (ANOVA) test revealed that particle size (p < 0.01) and Powder weight (p < 0.01) were the most influential parameters (ranked first and second), while solvent volume and time were less significant (p > 0.15). Findings using a linear regression model gave a yield variance of R² = 0.97. Confirmatory runs under optimized conditions reproduced the predicted yield within 0.2 % error. This approach comparatively delivers efficient oil recovery with minimal experimentation. Hence results from this study provides a robust basis for scaling up Delonix regia seed oil extraction in biodiesel and biosurfactant production.

Zenodo (CERN European Organization for Nuclear Research)
Igbinedion University (NG)
Openalex Percentile: Top 55%
Biodiesel Production and Applications
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Optimization of Delonix Regia Seed Oil Extraction using Taguchi Orthogonal Array Design · Zenodo (CERN European Organization for Nuclear Research) (2025) | TGRS Research Map | TGRS