A technical note on a compact inert-gas suitcase for optical measurements of air-sensitive 2D materials

We have designed and manufactured a low-cost, easy-to-use, inert-gas atmosphere over-pressurized compact suitcase for storing air-sensitive 2D materials or any other air-sensitive samples, as well as performing optical microscopy, Raman, and photoluminescence measurements. We demonstrate that the leaking rate of this suitcase is 1e-7 mbar.l/s, a low enough rate to protect an air-sensitive sample stored inside for at least 4.5 days. With Raman microscopy measurements, we further demonstrate that our inert-gas suitcase can protect Cr2Ge2Te3, a well-known air-sensitive 2D material for at least 8 days from degradation. In this technical note we share the details, operation and testing of this suitcase. We have also included the technical designs and the autodesk designs so that this design can be replicated by others who need such a system.

Institutions

Publication Details

Journal
Zenodo (CERN European Organization for Nuclear Research)
Published
2024-10-09
DOI
https://doi.org/10.5281/zenodo.13909565
Primary Topic
2D Materials and Applications
Type
article
Field-Weighted Citation Impact
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article

A technical note on a compact inert-gas suitcase for optical measurements of air-sensitive 2D materials

Zenodo (CERN European Organization for Nuclear Research)
2D Materials and Applications
article

A technical note on a compact inert-gas suitcase for optical measurements of air-sensitive 2D materials

article en

Abstract

We have designed and manufactured a low-cost, easy-to-use, inert-gas atmosphere over-pressurized compact suitcase for storing air-sensitive 2D materials or any other air-sensitive samples, as well as performing optical microscopy, Raman, and photoluminescence measurements. We demonstrate that the leaking rate of this suitcase is 1e-7 mbar.l/s, a low enough rate to protect an air-sensitive sample stored inside for at least 4.5 days. With Raman microscopy measurements, we further demonstrate that our inert-gas suitcase can protect Cr2Ge2Te3, a well-known air-sensitive 2D material for at least 8 days from degradation. In this technical note we share the details, operation and testing of this suitcase. We have also included the technical designs and the autodesk designs so that this design can be replicated by others who need such a system.

Zenodo (CERN European Organization for Nuclear Research)
Leiden University (NL)
Openalex Percentile: Top 74%
2D Materials and Applications
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A technical note on a compact inert-gas suitcase for optical measurements of air-sensitive 2D materials · Zenodo (CERN European Organization for Nuclear Research) (2024) | TGRS Research Map | TGRS