Development and validation of a portable adiabatic calorimeter based on cost-effective components

Adiabatic calorimetry is a widely recognised characterisation method that involves casting the studied material in a thermally isolated vessel, ensuring no energy exchange, and achieving so-called adiabatic conditions. This isolation enables the conduct of cement hydration without heat loss, ensuring consistent material characterisation independent of environmental conditions. Rigorous testing and validation were conducted to ensure compliance with the EN12390-15 standard for adiabatic calorimetry in concrete. Furthermore, a comparative analysis with a commercial adiabatic calorimeter demonstrated the reliability and accuracy of the proposed device in the characterization of mortar. This innovative device not only addresses the challenges of achieving adiabatic conditions in material characterisation but also provides a cost-effective and adaptable solution that can significantly benefit laboratories and industries engaged in research and development within the field.

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Publication Details

Journal
Zenodo (CERN European Organization for Nuclear Research)
Published
2024-11-12
DOI
https://doi.org/10.5281/zenodo.14778828
Primary Topic
Concrete and Cement Materials Research
Type
article
Field-Weighted Citation Impact
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article

Development and validation of a portable adiabatic calorimeter based on cost-effective components

Zenodo (CERN European Organization for Nuclear Research)
Concrete and Cement Materials Research
article

Development and validation of a portable adiabatic calorimeter based on cost-effective components

article en

Abstract

Adiabatic calorimetry is a widely recognised characterisation method that involves casting the studied material in a thermally isolated vessel, ensuring no energy exchange, and achieving so-called adiabatic conditions. This isolation enables the conduct of cement hydration without heat loss, ensuring consistent material characterisation independent of environmental conditions. Rigorous testing and validation were conducted to ensure compliance with the EN12390-15 standard for adiabatic calorimetry in concrete. Furthermore, a comparative analysis with a commercial adiabatic calorimeter demonstrated the reliability and accuracy of the proposed device in the characterization of mortar. This innovative device not only addresses the challenges of achieving adiabatic conditions in material characterisation but also provides a cost-effective and adaptable solution that can significantly benefit laboratories and industries engaged in research and development within the field.

Zenodo (CERN European Organization for Nuclear Research)
University of Minho (PT)
Industry, innovation and infrastructure
Openalex Percentile: Top 64%
Concrete and Cement Materials Research
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Development and validation of a portable adiabatic calorimeter based on cost-effective components · Zenodo (CERN European Organization for Nuclear Research) (2024) | TGRS Research Map | TGRS