Development and characterization of foam-mat freeze-dried beetroot powders: Role of carrier agents in foam behavior, powder functionality, and tablet formation

This study investigates the development of foam-mat freeze-dried beetroot powders and examines the role of carrier agents, maltodextrin and xanthan gum, on powder functionality and tablet formation. All formulations contained egg white albumen (5 wt%) as a foaming agent, while compositions varied based on the presence of maltodextrin (5 wt%) and xanthan gum at various concentrations (0.05, 0.1, or 0.2 wt%). Foams were prepared by whipping beetroot juice mixtures, followed by freeze-drying. The addition of maltodextrin slightly improved foam expansion (from ∼450 % to ∼460 %) and foam stability, whereas xanthan gum significantly increased the foam stability, with no drainage observed at 0.1 and 0.2 wt% within 180 min. However, foam expansion decreased to ∼370 % at 0.2 wt% xanthan gum content. Maltodextrin improved flowability (Hausner Ratio, HR: 1.29 vs. 1.32 for control) and reduced hygroscopicity (23.5 % vs. 26.0 %), while xanthan gum increased particle irregularity and cohesiveness, thus leading to higher HR values (up to 1.47) and poorer flow. The inclusion of xanthan gum also reduced powder solubility from ∼92 % down to ∼77 %. Kawakita analysis showed that maltodextrin and xanthan gum reduced plastic deformation and powder compactness. Tablets prepared from these powders exhibited reduced tensile strength and density compared to the control. Color analysis indicated that carrier addition increased lightness (L∗) and decreased redness (a∗), primarily due to pigment dilution and reduced compactness. • Red beetroot powders produced by foam-mat freeze-drying. • Maltodextrin improved foam stability, flow, and reduced hygroscopicity. • Xanthan gum enhanced foam stability but reduced solubility and flowability. • Maltodextrin reduced tablet strength, xanthan promoted partial strength recovery.

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Publication Details

Journal
Journal of Food Engineering
Published
2025-12-18
DOI
https://doi.org/10.1016/j.jfoodeng.2025.112934
Primary Topic
Microencapsulation and Drying Processes
Type
article
Field-Weighted Citation Impact
0.00

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article

Development and characterization of foam-mat freeze-dried beetroot powders: Role of carrier agents in foam behavior, powder functionality, and tablet formation

Rammile Ettelaie, Sherif M. Sherif, Amin Farshchi, Jabbar Gardy et al.
Journal of Food Engineering
Microencapsulation and Drying Processes
article

Development and characterization of foam-mat freeze-dried beetroot powders: Role of carrier agents in foam behavior, powder functionality, and tablet formation

Rammile Ettelaie, Sherif M. Sherif, Amin Farshchi, Jabbar Gardy, Vamsi Pavan Kumar Boddapati, Ali Hassnapour
article en

Abstract

This study investigates the development of foam-mat freeze-dried beetroot powders and examines the role of carrier agents, maltodextrin and xanthan gum, on powder functionality and tablet formation. All formulations contained egg white albumen (5 wt%) as a foaming agent, while compositions varied based on the presence of maltodextrin (5 wt%) and xanthan gum at various concentrations (0.05, 0.1, or 0.2 wt%). Foams were prepared by whipping beetroot juice mixtures, followed by freeze-drying. The addition of maltodextrin slightly improved foam expansion (from ∼450 % to ∼460 %) and foam stability, whereas xanthan gum significantly increased the foam stability, with no drainage observed at 0.1 and 0.2 wt% within 180 min. However, foam expansion decreased to ∼370 % at 0.2 wt% xanthan gum content. Maltodextrin improved flowability (Hausner Ratio, HR: 1.29 vs. 1.32 for control) and reduced hygroscopicity (23.5 % vs. 26.0 %), while xanthan gum increased particle irregularity and cohesiveness, thus leading to higher HR values (up to 1.47) and poorer flow. The inclusion of xanthan gum also reduced powder solubility from ∼92 % down to ∼77 %. Kawakita analysis showed that maltodextrin and xanthan gum reduced plastic deformation and powder compactness. Tablets prepared from these powders exhibited reduced tensile strength and density compared to the control. Color analysis indicated that carrier addition increased lightness (L∗) and decreased redness (a∗), primarily due to pigment dilution and reduced compactness. • Red beetroot powders produced by foam-mat freeze-drying. • Maltodextrin improved foam stability, flow, and reduced hygroscopicity. • Xanthan gum enhanced foam stability but reduced solubility and flowability. • Maltodextrin reduced tablet strength, xanthan promoted partial strength recovery.

Journal of Food EngineeringVol. 410
University of Leeds (GB), University of Bradford (GB), Teesside University (GB)
Teesside University
Openalex Percentile: Top 54%
Microencapsulation and Drying Processes
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