Enhancement of Wear Behaviour and Optimization and Prediction of Friction Coefficient of Nitrided D2 Steel at Different Times

The objective of this study is to evaluate the impact of thermal and thermochemical treatment, specifically gas nitriding, on the wear properties of AISI D2 cold work tool steel. The steel was austenitized at 1050 °C, then subjected to two annealing cycles at 560 °C for two hours each. It was then gas-nitrided for 16 and 36 h. The Vickers microhardness measurements of AISI D2 steel for the three distinct conditions, non-nitrided (NN), nitride at 16 h (N16) and nitride at 36 h (N36), are 560 HV0.1, 1050 HV0.1 and 1350 HV0.1, respectively. Wear tests were conducted utilizing a ball device, under dry friction conditions at ambient temperature, with loads of 5, 10 and 15 N, over 5000, 10,000 and 15,000 cycles at a constant sliding velocity of 30 mm/s and a sliding distance of 10 mm. Furthermore, the utilization of ANFIS modeling of experimental data facilitated the prediction of the variation in the coefficient of friction as a function of nitriding conditions and specific test parameters. The results show a significant effect of nitriding, leading to a marked reduction in the coefficient of friction. In the non-nitrided condition, the average value reaches 0.80, while extended nitriding to 36 h reduces this value to around 0.49, confirming a substantial tribological improvement. This enhancement is ascribed to the formation of hard, resilient nitride layers on the steel surface, thereby increasing wear resistance and cur-tailing in industrial applications.

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Publication Details

Journal
Lubricants
Published
2025-12-17
DOI
https://doi.org/10.3390/lubricants13120550
Primary Topic
Metal and Thin Film Mechanics
Type
article
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article

Enhancement of Wear Behaviour and Optimization and Prediction of Friction Coefficient of Nitrided D2 Steel at Different Times

Slah Mzali, Mohamed Ali Terres, Borhen Louhichi, Abdallah Souid
Lubricants
Metal and Thin Film Mechanics
article

Enhancement of Wear Behaviour and Optimization and Prediction of Friction Coefficient of Nitrided D2 Steel at Different Times

Slah Mzali, Mohamed Ali Terres, Borhen Louhichi, Abdallah Souid
article en

Abstract

The objective of this study is to evaluate the impact of thermal and thermochemical treatment, specifically gas nitriding, on the wear properties of AISI D2 cold work tool steel. The steel was austenitized at 1050 °C, then subjected to two annealing cycles at 560 °C for two hours each. It was then gas-nitrided for 16 and 36 h. The Vickers microhardness measurements of AISI D2 steel for the three distinct conditions, non-nitrided (NN), nitride at 16 h (N16) and nitride at 36 h (N36), are 560 HV0.1, 1050 HV0.1 and 1350 HV0.1, respectively. Wear tests were conducted utilizing a ball device, under dry friction conditions at ambient temperature, with loads of 5, 10 and 15 N, over 5000, 10,000 and 15,000 cycles at a constant sliding velocity of 30 mm/s and a sliding distance of 10 mm. Furthermore, the utilization of ANFIS modeling of experimental data facilitated the prediction of the variation in the coefficient of friction as a function of nitriding conditions and specific test parameters. The results show a significant effect of nitriding, leading to a marked reduction in the coefficient of friction. In the non-nitrided condition, the average value reaches 0.80, while extended nitriding to 36 h reduces this value to around 0.49, confirming a substantial tribological improvement. This enhancement is ascribed to the formation of hard, resilient nitride layers on the steel surface, thereby increasing wear resistance and cur-tailing in industrial applications.

LubricantsVol. 13(12)
University of Monastir (TN), Imam Mohammad ibn Saud Islamic University (SA), National Engineering School of Tunis (TN)
Openalex Percentile: Top 55%
Metal and Thin Film Mechanics
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