Design of Experiments Methodology for Fused Filament Fabrication of Silicon-Carbide-Particulate-Reinforced Polylactic Acid Composites

Fused Filament Fabrication (FFF) is an additive manufacturing technique that constructs parts by extruding material layer by layer. It offers advantages such as rapid prototyping, cost-effectiveness, and the ability to produce complex geometries. This study investigates the mechanical behavior of a composite filament composed of silicon carbide (SiC) ceramic particulates embedded in a polylactic acid (PLA) matrix, fabricated via FFF. Pure PLA specimens were also printed and tested to serve as a baseline. A Design of Experiments (DOE) methodology was employed to evaluate the influence of key printing parameters on mechanical properties, including Young’s modulus, yield strength, and ultimate strength. Microstructural analysis was performed on printed specimens using scanning electron microscopy (SEM). For compression testing, the parameters studied were infill percentage, number of shells, and print orientation. For tensile testing, the parameters included layer height, number of shells, and infill angle. Results indicated that infill percentage had the most significant impact on compressive properties, while layer height was the dominant factor in tensile performance. These findings provide insights into optimizing FFF process parameters for ceramic-particulate-reinforced polymer composites.

Authors

Institutions

Publication Details

Journal
Macromol—A Journal of Macromolecular Research
Published
2025-12-08
DOI
https://doi.org/10.3390/macromol5040060
Citations
1
Primary Topic
Additive Manufacturing and 3D Printing Technologies
Type
article
Field-Weighted Citation Impact
0.68

Funders

Controls
|||
ALL TIME
JAN
FEB
MAR
APR
MAY
JUN
JUL
AUG
SEP
OCT
article

Design of Experiments Methodology for Fused Filament Fabrication of Silicon-Carbide-Particulate-Reinforced Polylactic Acid Composites

Michael C. Halbig, Andrew L. Gyekenyesi, Mrityunjay Singh, Meelad Ranaiefar
1 citations
Macromol—A Journal of Macromolecular Research
Additive Manufacturing and 3D Printing Technologies
0.68
article

Design of Experiments Methodology for Fused Filament Fabrication of Silicon-Carbide-Particulate-Reinforced Polylactic Acid Composites

Michael C. Halbig, Andrew L. Gyekenyesi, Mrityunjay Singh, Meelad Ranaiefar
article en
1 citations

Abstract

Fused Filament Fabrication (FFF) is an additive manufacturing technique that constructs parts by extruding material layer by layer. It offers advantages such as rapid prototyping, cost-effectiveness, and the ability to produce complex geometries. This study investigates the mechanical behavior of a composite filament composed of silicon carbide (SiC) ceramic particulates embedded in a polylactic acid (PLA) matrix, fabricated via FFF. Pure PLA specimens were also printed and tested to serve as a baseline. A Design of Experiments (DOE) methodology was employed to evaluate the influence of key printing parameters on mechanical properties, including Young’s modulus, yield strength, and ultimate strength. Microstructural analysis was performed on printed specimens using scanning electron microscopy (SEM). For compression testing, the parameters studied were infill percentage, number of shells, and print orientation. For tensile testing, the parameters included layer height, number of shells, and infill angle. Results indicated that infill percentage had the most significant impact on compressive properties, while layer height was the dominant factor in tensile performance. These findings provide insights into optimizing FFF process parameters for ceramic-particulate-reinforced polymer composites.

Macromol—A Journal of Macromolecular ResearchVol. 5(4)
Cleveland State University (US), Glenn Research Center (US), Ohio Aerospace Institute (US)
National Aeronautics and Space Administration, Ohio Space Grant Consortium
Openalex Percentile: Top 23%
Additive Manufacturing and 3D Printing Technologies
0.68
AI Navigator

Ask Laika to Summarize, Analyze, and Connect papers live on the map.

Summarize Papers & Methodologies

Extract key findings, datasets, and comparative methods across publications.

Benchmark Rankings & Visual Analytics

Rank top research institutions, authors, funders, topics, and journals by Field-Weighted Citation Impact (FWCI) and paper volume with instant charts.

Connect Distant Disciplines

Bridge topological clusters on the map to find hidden collaborative intersections.

Design of Experiments Methodology for Fused Filament Fabrication of Silicon-Carbide-Particulate-Reinforced Polylactic Acid Composites — Michael C. Halbig, Andrew L. Gyekenyesi, et al. · Macromol—A Journal of Macromolecular Research (2025) | TGRS Research Map | TGRS