Comprehensive investigation of a novel PLA/EPDM/TiO <sub>2</sub> /CNT nanocomposite produced by selective laser sintering

This study aims to enhance the electrical, mechanical, and thermal properties of a novel PLA/EPDM/TiO 2 /CNT nanocomposite fabricated by selective laser sintering (SLS). For this purpose, the response surface method (RSM) was employed to examine the effect of the process parameters such as laser power, scan rate, CNTs, and TiO 2 nanoparticles on the melting temperature, crystallization temperature, electrical conductivity, tensile stress, and impact resistance of the nanocomposite. Thermal characterization was conducted via TGA and DSC, whereas electrical and microstructural properties were assessed using a four-probe test and SEM imaging. The results indicate that incorporating CNT and TiO 2 nanoparticles significantly enhanced the material’s thermal stability and electrical conductivity. A homogeneous distribution of nanoparticles within the microstructure was achieved with a 2 wt% concentration of CNT and TiO 2 . Furthermore, minimal porosity and effective solidification were obtained at a laser power of 18 W and a scan rate of 2500 mm/s. The optimization process using RSM and desirability function analysis determined that the optimal parameters for simultaneously improving tensile stress and impact resistance were: 1.8 wt% CNT, 1.9 wt% TiO 2 , a laser power of 16.5 W, and a scan rate of 2624 mm/s.

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Publication Details

Journal
Journal of Thermoplastic Composite Materials
Published
2025-11-26
DOI
https://doi.org/10.1177/08927057251403537
Primary Topic
Additive Manufacturing and 3D Printing Technologies
Type
article
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article

Comprehensive investigation of a novel PLA/EPDM/TiO 2 /CNT nanocomposite produced by selective laser sintering

Ishraga GalalEldin Abdalla Awad
Journal of Thermoplastic Composite Materials
Additive Manufacturing and 3D Printing Technologies
article

Comprehensive investigation of a novel PLA/EPDM/TiO 2 /CNT nanocomposite produced by selective laser sintering

Ishraga GalalEldin Abdalla Awad
article en

Abstract

This study aims to enhance the electrical, mechanical, and thermal properties of a novel PLA/EPDM/TiO 2 /CNT nanocomposite fabricated by selective laser sintering (SLS). For this purpose, the response surface method (RSM) was employed to examine the effect of the process parameters such as laser power, scan rate, CNTs, and TiO 2 nanoparticles on the melting temperature, crystallization temperature, electrical conductivity, tensile stress, and impact resistance of the nanocomposite. Thermal characterization was conducted via TGA and DSC, whereas electrical and microstructural properties were assessed using a four-probe test and SEM imaging. The results indicate that incorporating CNT and TiO 2 nanoparticles significantly enhanced the material’s thermal stability and electrical conductivity. A homogeneous distribution of nanoparticles within the microstructure was achieved with a 2 wt% concentration of CNT and TiO 2 . Furthermore, minimal porosity and effective solidification were obtained at a laser power of 18 W and a scan rate of 2500 mm/s. The optimization process using RSM and desirability function analysis determined that the optimal parameters for simultaneously improving tensile stress and impact resistance were: 1.8 wt% CNT, 1.9 wt% TiO 2 , a laser power of 16.5 W, and a scan rate of 2624 mm/s.

Journal of Thermoplastic Composite Materials
University of Hafr Al-Batin (SA)
Openalex Percentile: Top 60%
Additive Manufacturing and 3D Printing Technologies
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