Mechanical properties of ECC incorporated with micro-powder of construction waste after elevated-temperature exposure

• 20 % MPCW lowers ECC strength by 13 % yet still satisfies the ≤25 % loss criterion. • Above 400 °C both ECC and MPCW-ECC drop below 75 % of original strength, breaching specifications. • Beyond 300 °C both materials turn brittle; multi-crack capacity and toughness vanish. • XRD shows MPCW shifts peaks and weakens phase stability; hydrate decomposition drives macro-deterioration. • SEM shows MPCW accelerates micro-damage; ITZ becomes the high-temperature failure path. • Linear models confirm temperature as the dominant strength suppressor. With the increasing demand for resource utilization of construction waste and advancing research on the elevated-temperature behavior of engineering materials, incorporating micro-powder of construction waste (MPCW) into engineered cementitious composites (ECC) and studying their mechanical properties under elevated temperatures are of great practical value. This study investigates the mechanical behavior of ECC where natural aggregates are partially replaced by MPCW, within the temperature range of 20 °C to 600 °C, with control groups including ECC without MPCW and ECC with 20 % MPCW substitution. Results show that MPCW incorporation reduces ECC strength, but the compressive strength loss (13.34 %) meets the engineering design standard (maximum allowed loss<25 %). As temperature rises, the compressive, tensile, and flexural tensile strengths of MPCW-ECC, along with their corresponding strains, first increase and then decrease. When the temperature exceeds 300 °C, the failure mode becomes more brittle, and flexural failure no longer follows the multi-cracking mechanism; above 400 °C, its compressive strength drops to <75 % of the control group. X-ray diffraction (XRD) analysis reveals that the crystal phase transformations of ECC and MPCW-ECC matrices at different temperatures are highly consistent with macroscopic performance trends, while scanning electron microscopy (SEM) further clarifies the microstructural evolution and its impact on mechanical behavior. Additionally, a regression model established for MPCW-ECC mechanical properties shows high predictive accuracy, with R² values of 0.911, 0.880, and 0.865 for compressive, tensile, and flexural tensile strengths, respectively. Overall, this study provides a scientific basis for the elevated-temperature safety evaluation of MPCW-ECC and valuable insights into the sustainable utilization of construction waste in cement-based composites.

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Publication Details

Journal
Results in Engineering
Published
2025-11-20
DOI
https://doi.org/10.1016/j.rineng.2025.108304
Primary Topic
Innovative concrete reinforcement materials
Type
article
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article

Mechanical properties of ECC incorporated with micro-powder of construction waste after elevated-temperature exposure

Shu Wan, Ming Ma, Songqiang Wan, Xiaoze Yang et al.
Results in Engineering
Innovative concrete reinforcement materials
article

Mechanical properties of ECC incorporated with micro-powder of construction waste after elevated-temperature exposure

Shu Wan, Ming Ma, Songqiang Wan, Xiaoze Yang, Chenjie Hao, Jiahong Dai, Liang Cui, Yu Hao Wang, Hongbo Xiao, Ziyi Song, Long Liu, Chong Liu, Chunling Yan, Yingying Bi
article en

Abstract

• 20 % MPCW lowers ECC strength by 13 % yet still satisfies the ≤25 % loss criterion. • Above 400 °C both ECC and MPCW-ECC drop below 75 % of original strength, breaching specifications. • Beyond 300 °C both materials turn brittle; multi-crack capacity and toughness vanish. • XRD shows MPCW shifts peaks and weakens phase stability; hydrate decomposition drives macro-deterioration. • SEM shows MPCW accelerates micro-damage; ITZ becomes the high-temperature failure path. • Linear models confirm temperature as the dominant strength suppressor. With the increasing demand for resource utilization of construction waste and advancing research on the elevated-temperature behavior of engineering materials, incorporating micro-powder of construction waste (MPCW) into engineered cementitious composites (ECC) and studying their mechanical properties under elevated temperatures are of great practical value. This study investigates the mechanical behavior of ECC where natural aggregates are partially replaced by MPCW, within the temperature range of 20 °C to 600 °C, with control groups including ECC without MPCW and ECC with 20 % MPCW substitution. Results show that MPCW incorporation reduces ECC strength, but the compressive strength loss (13.34 %) meets the engineering design standard (maximum allowed loss<25 %). As temperature rises, the compressive, tensile, and flexural tensile strengths of MPCW-ECC, along with their corresponding strains, first increase and then decrease. When the temperature exceeds 300 °C, the failure mode becomes more brittle, and flexural failure no longer follows the multi-cracking mechanism; above 400 °C, its compressive strength drops to <75 % of the control group. X-ray diffraction (XRD) analysis reveals that the crystal phase transformations of ECC and MPCW-ECC matrices at different temperatures are highly consistent with macroscopic performance trends, while scanning electron microscopy (SEM) further clarifies the microstructural evolution and its impact on mechanical behavior. Additionally, a regression model established for MPCW-ECC mechanical properties shows high predictive accuracy, with R² values of 0.911, 0.880, and 0.865 for compressive, tensile, and flexural tensile strengths, respectively. Overall, this study provides a scientific basis for the elevated-temperature safety evaluation of MPCW-ECC and valuable insights into the sustainable utilization of construction waste in cement-based composites.

Results in EngineeringVol. 28
Shijiazhuang University (CN), Zhong Ke San Huan (China) (CN), Ningxia Water Conservancy (CN), Anyang Institute of Technology (CN), Henan Polytechnic University (CN), Northeast Forestry University (CN), Chongqing Jiaotong University (CN), Shijiazhuang Tiedao University (CN)
Openalex Percentile: Top 63%
Innovative concrete reinforcement materials
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