Variations in mechanical, electrical, thermal properties, and residual stress of laser powder bed fused Al–Fe binary alloy by annealing

Al–2.5 mass% Fe binary alloys were prepared by laser powder bed fusion (L-PBF), and the effects of annealing below 573 K on the electrical, mechanical, thermal properties, microstructure, and residual stress were investigated. The electrical resistivity of the L-PBF alloy remained almost unchanged after annealing at 473 K, while that of the specimen annealed at 573 K decreased from 20 to 8 nΩ m and from 47 to 37 nΩ m at 77 K and 293 K, respectively. Vickers hardness (measured on the surface normal to the building direction) increased to about 102 HV from 97 HV, then decreased to 94 HV during annealing at 573 K, showing a similar trend on the parallel surface. These hardness changes agreed with the formation of nanoscale Al 6 Fe precipitates, corresponding to a decrease in solute Fe concentration of about 0.47–0.52 mass% estimated from electrical resistivity and X-ray diffraction. Compression tests revealed no anisotropy in the 0.2 % proof stress between as-built and annealed specimens. Residual stress was effectively removed by annealing at 573 K for >120 s. Annealing also increased the specific heat from 800 to 920 J/(kg·K), attributed to reduced solute Fe and an increased Al 6 Fe fraction. The measured thermal conductivities agreed well with reported values.

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Publication Details

Journal
Journal of Materials Research and Technology
Published
2025-11-01
DOI
https://doi.org/10.1016/j.jmrt.2025.11.107
Primary Topic
Additive Manufacturing Materials and Processes
Type
article
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article

Variations in mechanical, electrical, thermal properties, and residual stress of laser powder bed fused Al–Fe binary alloy by annealing

Yoji Miyajima, Ryota Tatsumi, Toshihiko Sasaki, Kayoko Yanagi et al.
Journal of Materials Research and Technology
Additive Manufacturing Materials and Processes
article

Variations in mechanical, electrical, thermal properties, and residual stress of laser powder bed fused Al–Fe binary alloy by annealing

Yoji Miyajima, Ryota Tatsumi, Toshihiko Sasaki, Kayoko Yanagi, Kazuhiro Ishikawa, Naoki Takata, Dasom Kim, Y. Hamasaki, Hiroki Adachi
article en

Abstract

Al–2.5 mass% Fe binary alloys were prepared by laser powder bed fusion (L-PBF), and the effects of annealing below 573 K on the electrical, mechanical, thermal properties, microstructure, and residual stress were investigated. The electrical resistivity of the L-PBF alloy remained almost unchanged after annealing at 473 K, while that of the specimen annealed at 573 K decreased from 20 to 8 nΩ m and from 47 to 37 nΩ m at 77 K and 293 K, respectively. Vickers hardness (measured on the surface normal to the building direction) increased to about 102 HV from 97 HV, then decreased to 94 HV during annealing at 573 K, showing a similar trend on the parallel surface. These hardness changes agreed with the formation of nanoscale Al 6 Fe precipitates, corresponding to a decrease in solute Fe concentration of about 0.47–0.52 mass% estimated from electrical resistivity and X-ray diffraction. Compression tests revealed no anisotropy in the 0.2 % proof stress between as-built and annealed specimens. Residual stress was effectively removed by annealing at 573 K for >120 s. Annealing also increased the specific heat from 800 to 920 J/(kg·K), attributed to reduced solute Fe and an increased Al 6 Fe fraction. The measured thermal conductivities agreed well with reported values.

Journal of Materials Research and TechnologyVol. 39
Kanazawa University (JP), University of Hyogo (JP), Japan Synchrotron Radiation Research Institute (JP), Nagoya University (JP)
Openalex Percentile: Top 63%
Additive Manufacturing Materials and Processes
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