Using a Combination of ECAP and HE Processes to Produce Isotropic Ultrafine-Grained Titanium

This paper proposes a complex plastic forming process for grade 2 titanium using a combination of severe plastic deformation techniques, equal-channel angular pressing (ECAP) and hydrostatic extrusion (HE). The aim of the combination of these methods is to reduce the strength of the phenomenon of microstructural anisotropy and the resulting anisotropy of mechanical properties characteristic of the HE process. Two routes of plastic deformation (HE and ECAP + HE) were compared using the same total strain rate of ε ~ 3.5. Results: The analysis of mechanical properties and microstructure studies using TEM and SEM/EBSD techniques showed that it is possible to obtain large microstructure refinement of titanium with almost identical mechanical properties via both studied techniques. In addition, this also leads to a significant improvement in the strength of UTS by ~ 1000 MPa, YS by ~ 945 MPa and ductility (E) by ~ 25%. These findings indicate that applying a sequential ECAP + HE strategy can effectively reduce anisotropy and improve the overall performance of grade 2 titanium.

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Publication Details

Journal
Materials
Published
2025-11-15
DOI
https://doi.org/10.3390/ma18225194
Citations
1
Primary Topic
Microstructure and mechanical properties
Type
article
Field-Weighted Citation Impact
0.52
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article

Using a Combination of ECAP and HE Processes to Produce Isotropic Ultrafine-Grained Titanium

Łukasz Maj, Mariusz Kulczyk, Jacek Skiba, Jakub Kawałko et al.
1 citations
Materials
Microstructure and mechanical properties
0.52
article

Using a Combination of ECAP and HE Processes to Produce Isotropic Ultrafine-Grained Titanium

Łukasz Maj, Mariusz Kulczyk, Jacek Skiba, Jakub Kawałko, Sylwia Przybysz, Monika Skorupska
article en
1 citations

Abstract

This paper proposes a complex plastic forming process for grade 2 titanium using a combination of severe plastic deformation techniques, equal-channel angular pressing (ECAP) and hydrostatic extrusion (HE). The aim of the combination of these methods is to reduce the strength of the phenomenon of microstructural anisotropy and the resulting anisotropy of mechanical properties characteristic of the HE process. Two routes of plastic deformation (HE and ECAP + HE) were compared using the same total strain rate of ε ~ 3.5. Results: The analysis of mechanical properties and microstructure studies using TEM and SEM/EBSD techniques showed that it is possible to obtain large microstructure refinement of titanium with almost identical mechanical properties via both studied techniques. In addition, this also leads to a significant improvement in the strength of UTS by ~ 1000 MPa, YS by ~ 945 MPa and ductility (E) by ~ 25%. These findings indicate that applying a sequential ECAP + HE strategy can effectively reduce anisotropy and improve the overall performance of grade 2 titanium.

MaterialsVol. 18(22)
Institute of High Pressure Physics (PL), Institute of Metallurgy and Materials Science (PL), AGH University of Krakow (PL), Polish Academy of Sciences (PL)
Openalex Percentile: Top 30%
Microstructure and mechanical properties
0.52
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